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1-BROMO-2,4,6-TRIISOPROPYLBENZENE

Product Name 1-BROMO-2,4,6-TRIISOPROPYLBENZENE

CAS21524-34-5

MFC15H23Br

MW283.25

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  • Mass 

    MS-NW-6118          
2-bromo-1,3,5-triisopropylbenzene
C15H23Br            (Mass of molecular ion:    282)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          15.0       1.0
      27.0       8.6
      29.0       3.3
      39.0       6.1
      41.0      22.8
      42.0       1.0
      43.0      89.4
      44.0       3.0
      50.0       1.1
      51.0       4.3
      52.0       1.2
      53.0       3.4
      55.0       2.6
      63.0       3.1
      64.0       3.9
      65.0       3.8
      67.0       1.5
      70.0       1.5
      70.5       1.5
      71.0       3.0
      72.0       1.0
      75.0       1.5
      76.0       2.7
      77.0       7.5
      77.5       1.0
      78.0       2.9
      79.0       2.8
      89.0       1.4
      91.0      14.8
      92.0       1.5
     102.0       1.5
     103.0       2.7
     104.0       2.2
     105.0       6.5
     111.0       1.6
     112.0       1.5
     115.0      10.4
     116.0       4.8
     117.0      12.6
     118.0       4.2
     119.0       4.5
     126.0       1.7
     127.0       4.3
     128.0      10.3
     129.0       9.5
     130.0       5.7
     131.0       8.0
     132.0       2.0
     133.0       2.1
     141.0       4.9
     142.0       3.6
     143.0       4.8
     144.0       3.1
     145.0      10.3
     146.0       5.4
     147.0       1.7
     153.0       1.2
     155.0       1.3
     156.0       1.0
     157.0       2.4
     158.0       1.1
     159.0       6.8
     160.0       1.8
     169.0       1.9
     171.0       1.8
     173.0       3.5
     175.0       1.2
     183.0       2.8
     185.0       2.6
     187.0       2.1
     188.0       1.3
     197.0       2.2
     199.0       1.8
     203.0       8.4
     204.0       1.7
     211.0       4.0
     213.0       3.5
     225.0       7.7
     226.0       1.2
     227.0       6.8
     228.0       1.1
     239.0      12.7
     240.0       2.1
     241.0      12.4
     242.0       2.0
     253.0       5.4
     254.0       1.2
     255.0       4.9
     256.0       1.1
     267.0      99.6
     268.0      17.8
     269.0     100.0
     270.0      17.2
     271.0       1.5
     282.0      43.5
     283.0       8.0
     284.0      42.4
     285.0       7.6

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C15 H23 Br 0.05 ml : 0.5 ml CDCl3
    2-bromo-1,3,5-triisopropylbenzene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.985
      B             3.487
      C             2.862
      D             1.242
      E             1.240
  

         Hz     ppm     Int.


       2791.63   6.986    369
   1407.47   3.522     38
   1400.63   3.505     94
   1393.80   3.488    127
   1386.96   3.471     98
   1380.13   3.454     41
   1151.12   2.881     41
   1144.17   2.863     57
   1137.21   2.846     44
    500.12   1.252   1000
    499.15   1.249    842
    493.16   1.234    988
    492.07   1.232    886

in CDCl3



liquid film



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