2-Chlorobenzotrichloride

Mass

MS-NW-1073          
alpha,alpha,alpha,2-tetrachlorotoluene
C7H4Cl4             (Mass of molecular ion:    228)

   Source Temperature: 240 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      18.0       1.3
      35.0       1.3
      36.0       2.8
      37.0       1.7
      38.0       1.5
      39.0       3.4
      43.0       3.5
      49.0       1.5
      50.0       3.5
      51.0       1.5
      60.0       2.1
      61.0      10.3
      62.0       6.8
      63.0       4.7
      72.0       1.3
      73.0       7.7
      74.0       1.7
      75.0       2.8
      78.0       1.2
      78.5       2.3
      79.0       4.2
      79.5       2.0
      80.0       2.2
      84.0       1.8
      85.0       2.1
      86.0       2.9
      87.0       4.3
      88.0       1.7
      96.0       2.9
      96.5       6.2
      97.0       6.2
      97.5       6.2
      98.0       1.7
      98.5       1.9
      99.0       2.2
     107.0       1.6
     109.0       1.3
     123.0      22.0
     124.0       2.3
     125.0       6.9
     133.0       2.4
     135.0       1.4
     157.0       4.1
     158.0       7.4
     159.0       7.2
     160.0       5.4
     161.0       3.4
     162.0       1.0
     176.0       1.6
     193.0     100.0
     194.0       8.3
     195.0      95.7
     196.0       8.1
     197.0      31.1
     198.0       2.6
     199.0       3.5
     228.0       6.8
     229.0       1.2
     230.0       8.6
     231.0       1.0
     232.0       4.1
     246.0       5.2
     248.0       3.2
     316.0       1.1
     318.0       1.6

Parameter ppm Hz D(A) 8.14 D(B) 7.27 D(C) 7.31 D(D) 7.48 J(A,B) 7.43 J(A,C) 1.84 J(A,D) 0.31 J(B,C) 7.06 J(B,D) 1.25 J(C,D) 7.71 SMITH,W.B. ET AL. J.PHYS.CHEM. 74, 812 (1970)

     Hz     ppm     Int.

   2453.06   8.177     12
   2446.69   8.156    516
   2444.70   8.149    387
   2444.07   8.147    377
   2439.74   8.132    624
   2437.43   8.125    552
   2430.73   8.102     13
   2248.78   7.496    451
   2247.03   7.490    548
   2241.87   7.473    427
   2241.25   7.471    458
   2239.83   7.466    634
   2232.88   7.443     19
   2201.97   7.340    193
   2199.86   7.333    239
   2194.93   7.316    589
   2192.79   7.309    547
   2187.87   7.293   1000
   2185.83   7.286    716
   2180.73   7.269    598
   2179.12   7.264    518
   2173.66   7.246    198
   2172.11   7.240    157