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MassMS2004-02556WA 2-azidonaphthalene C10H7N3 (Mass of molecular ion: 169)
Source Temperature: 100 °C Sample Temperature: 90 °C Direct, 70 eV
27.0 2.0 28.0 3.8 37.0 2.4 38.0 5.3 39.0 10.9 50.0 9.7 51.0 9.8 52.0 2.3 56.0 1.1 56.5 2.6 57.0 5.9 57.5 5.6 61.0 4.1 62.0 11.3 63.0 18.6 64.0 5.5 65.0 2.2 69.5 1.1 70.0 1.9 70.5 21.6 71.0 2.5 74.0 5.7 75.0 5.7 76.0 2.9 77.0 2.2 85.0 1.3 86.0 3.4 87.0 6.6 88.0 10.1 89.0 4.2 90.0 2.1 98.0 1.0 99.0 1.0 112.0 1.0 113.0 15.0 114.0 43.1 115.0 9.5 126.0 1.0 127.0 1.5 139.0 1.8 140.0 59.5 141.0 100.0 142.0 11.3 143.0 1.8 169.0 43.5 170.0 5.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C10H7N3 40 mg : 0.5 ml CDCl3 2-azidonaphthalene 
Assign. Shift(ppm)
A 7.781 B *1 7.773 C *1 7.717 D *2 7.461 E 7.410 F *2 7.406 G 7.119
Hz ppm Int.3115.12 7.793 1000 3111.70 7.784 691 3110.97 7.782 687 3103.52 7.764 736 3102.91 7.762 721 3089.60 7.729 636 3088.99 7.727 653 3081.55 7.709 719 3080.82 7.707 734 2991.34 7.483 385 2990.00 7.480 422 2984.38 7.465 668 2983.16 7.462 855 2981.82 7.459 393 2976.32 7.445 621 2974.98 7.442 566 2966.68 7.421 770 2965.34 7.418 866 2958.50 7.401 958 2951.79 7.384 376 2950.44 7.381 361 2851.32 7.133 941 2849.00 7.127 894 2842.53 7.111 873 2840.34 7.105 825
in CDCl3
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