3-Fluorocinnamic acid

Mass

MS-NW-9396          
trans-3-fluorocinnamic acid
C9H7FO2             (Mass of molecular ion:    166)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       2.5
      27.0       1.0
      28.0       1.8
      31.0       1.0
      38.0       1.0
      39.0       2.6
      45.0       3.2
      50.0       6.7
      50.5       2.6
      51.0       7.6
      55.0       1.8
      57.0       2.9
      59.0       1.2
      60.0       6.9
      60.5       4.4
      61.0       1.6
      62.0       2.0
      63.0       3.7
      68.0       2.2
      69.0       5.3
      70.0       4.0
      71.0       1.9
      73.0       2.1
      74.0       6.3
      74.5       2.4
      75.0      20.9
      76.0       2.2
      77.0       1.1
      81.0       2.1
      83.0       4.8
      92.0       1.0
      93.0       1.7
      94.0       5.5
      95.0      10.4
      96.0       5.1
      97.0       3.4
      98.0       1.5
      99.0       2.3
     100.0       2.1
     101.0      46.3
     102.0       4.7
     107.0       1.0
     109.0      21.0
     110.0       3.6
     112.0       1.5
     118.0       3.4
     119.0       1.4
     120.0      21.6
     121.0      38.8
     122.0       4.0
     123.0       2.1
     124.0       1.1
     125.0       2.6
     137.0       4.7
     138.0       9.9
     147.0       5.7
     148.0       5.0
     149.0      35.1
     150.0       3.5
     165.0      77.8
     166.0     100.0
     167.0      10.2

Assign. Shift(ppm) A 12.55 B 7.62 C 7.62 D 7.544 E 7.471 G 7.258 J 6.640 J(B,J)=16.0HZ

     Hz     ppm     Int.

   5016.02  12.552    190
   3052.90   7.639    881
   3049.49   7.631    349
   3040.51   7.608    373
   3036.88   7.599    751
   3019.78   7.557    387
   3012.09   7.537    630
   2996.71   7.499    264
   2990.72   7.484    287
   2988.59   7.479    437
   2982.60   7.464    416
   2980.89   7.459    283
   2977.05   7.450     36
   2974.70   7.444    203
   2910.38   7.283    217
   2908.67   7.279    194
   2907.81   7.276    205
   2901.62   7.261    357
   2899.69   7.256    347
   2893.28   7.240    187
   2891.57   7.236    163
   2890.93   7.234    167
   2661.44   6.660   1000
   2645.41   6.620    918