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MassMS-KW-0501 5-bromoacenaphthene C12H9Br (Mass of molecular ion: 232)
Source Temperature: 120 °C Sample Temperature: 100 °C Direct, 75 eV
39.0 1.3 50.0 2.5 51.0 2.8 61.0 1.1 62.0 3.5 63.0 12.9 63.5 1.8 74.0 4.1 75.0 10.9 75.5 12.3 76.0 41.5 76.5 21.0 77.0 4.4 86.0 1.7 87.0 2.0 98.0 2.1 99.0 1.9 100.0 1.0 101.0 1.3 102.0 1.0 116.0 2.8 117.0 2.5 125.0 1.6 126.0 3.7 127.0 1.9 149.0 1.0 150.0 10.8 151.0 20.8 152.0 65.7 153.0 100.0 154.0 13.1 231.0 2.2 232.0 66.8 233.0 10.9 234.0 65.1 235.0 8.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H9 Br 0.034 g : 0.5 ml CDCl3 5-bromoacenaphthene 
Assign. Shift(ppm)
A 7.742 B 7.621 C 7.514 D 7.287 E 7.087 F 3.37 G 3.29
Hz ppm Int.3099.00 7.755 468 3098.27 7.753 500 3090.58 7.734 570 3089.97 7.732 604 3049.68 7.631 928 3046.26 7.623 72 3042.36 7.613 1000 3010.50 7.533 522 3007.32 7.525 77 3003.54 7.516 609 3002.20 7.513 491 2995.24 7.495 510 2915.28 7.295 485 2908.45 7.278 431 2837.40 7.100 302 2836.06 7.097 612 2834.59 7.093 356 2829.96 7.082 292 2828.61 7.078 581 2827.27 7.075 336 1354.74 3.390 307 1353.52 3.387 326 1349.00 3.376 542 1346.19 3.369 363 1344.85 3.366 390 1343.38 3.362 441 1341.92 3.358 617 1340.94 3.356 628 1320.31 3.304 750 1319.09 3.301 511 1317.63 3.297 437 1316.28 3.294 412 1314.70 3.290 356 1313.23 3.286 556 1312.26 3.284 534 1308.96 3.276 282 1307.62 3.272 411 1306.27 3.269 280
in CDCl3
KBr disc
nujol mull
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