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2,6-Dichlorobenzyl bromide

Product Name 2,6-Dichlorobenzyl bromide

CAS20443-98-5

MFC7H5BrCl2

MW239.92

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  • Mass 

    MS-NW-7264          
alpha-bromo-2,6-dichlorotoluene
C7H5BrCl2           (Mass of molecular ion:    238)


       Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          37.0       1.9
      38.0       2.0
      39.0       4.2
      43.0       2.9
      43.5       1.1
      44.0       3.8
      49.0       1.3
      50.0       3.2
      51.0       2.3
      61.0       5.0
      61.5       4.1
      62.0       9.8
      62.5       1.5
      63.0      12.4
      73.0       5.9
      74.0       1.1
      75.0       2.1
      79.5       5.7
      80.5       3.6
      84.0       1.2
      85.0       1.5
      86.0       2.3
      87.0       3.1
      88.0       1.4
      89.0      13.5
      90.0       1.0
      97.0       2.3
      99.0       2.9
     101.0       1.2
     123.0      11.5
     124.0       5.9
     125.0       4.9
     126.0       2.0
     133.0       2.5
     135.0       1.6
     159.0     100.0
     160.0       8.1
     161.0      62.9
     162.0       5.3
     163.0      10.2
     238.0       4.2
     240.0       6.5
     242.0       2.9

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C7 H5 Br Cl2 0.039 g : 0.5 ml CDCl3
    alpha-bromo-2,6-dichlorotoluene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.321
      B             7.185
      C             4.758
  

         Hz     ppm     Int.


       2930.54   7.333    352
   2922.61   7.313    558
   2878.42   7.203    239
   2870.97   7.184    197
   2869.75   7.181    181
   2862.30   7.163    139
   1901.86   4.759   1000

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder



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