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MassMS-NW-6198 3-acetylphenanthrene C16H12O (Mass of molecular ion: 220)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 2.8 43.0 4.4 51.0 1.1 62.0 1.0 63.0 1.5 74.0 1.9 75.0 4.3 76.0 1.0 82.5 1.1 87.0 2.4 87.5 1.5 88.0 19.0 88.5 7.8 89.0 1.5 94.5 1.9 95.0 1.0 96.0 2.7 98.0 1.2 99.0 1.1 102.5 5.7 103.0 1.1 110.0 1.5 126.0 1.1 149.0 1.2 150.0 5.8 151.0 11.7 152.0 2.1 174.0 2.8 175.0 4.3 176.0 29.1 177.0 50.4 178.0 8.4 189.0 2.7 190.0 1.0 191.0 1.5 205.0 100.0 206.0 17.0 207.0 1.6 220.0 80.9 221.0 14.3 222.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H12 O 0.041 g : 0.5 ml CDCl3 3-acetylphenanthrene 
Assign. Shift(ppm)
A 9.230 B 8.704 C 8.071 D 7.86 E 7.855 F 7.782 G 7.680 J 7.68 K 7.609 L 2.739 ASSIGNEG BY H-H COSY.
Hz ppm Int.3689.45 9.232 113 3688.48 9.230 116 3483.64 8.717 69 3483.15 8.716 71 3475.46 8.697 71 3474.85 8.695 73 3230.96 8.085 84 3229.25 8.081 87 3222.66 8.064 103 3220.95 8.060 105 3147.09 7.875 66 3146.36 7.873 67 3142.94 7.865 139 3140.01 7.857 85 3138.55 7.854 84 3134.64 7.844 114 3115.48 7.796 82 3106.69 7.774 123 3073.12 7.690 154 3067.50 7.676 67 3066.16 7.673 87 3064.82 7.669 115 3059.33 7.656 62 3057.86 7.652 58 3047.85 7.627 68 3046.51 7.623 74 3040.77 7.609 52 3039.92 7.607 77 3038.82 7.604 72 3032.96 7.590 38 3031.74 7.586 36 1094.73 2.740 1000
in CDCl3
KBr disc
nujol mull
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