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MS-NW-1222 4-(2-aminoethyl)morpholine C6H14N2O (Mass of molecular ion: 130)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 5.7 18.0 2.9 27.0 3.5 28.0 11.0 29.0 5.5 30.0 14.1 41.0 3.6 42.0 9.4 43.0 5.6 44.0 6.3 45.0 1.3 54.0 1.2 55.0 1.2 56.0 29.0 57.0 2.6 58.0 1.0 70.0 6.4 71.0 1.2 72.0 2.6 84.0 1.2 86.0 1.2 88.0 1.4 100.0 100.0 101.0 6.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H14 N2 O 0.04 ml : 0.5 ml CDCl3 4-(2-aminoethyl)morpholine Assign. Shift(ppm)
A 3.706 B 2.783 C 2.45 D 2.42 E 1.37
Hz ppm Int.
336.81 3.761 363 333.81 3.728 184 332.25 3.710 338 330.25 3.688 185 327.38 3.656 410 257.00 2.870 99 255.75 2.856 105 251.19 2.805 158 250.44 2.797 233 244.69 2.733 228 243.94 2.724 208 223.81 2.499 414 222.38 2.484 311 221.56 2.474 346 219.00 2.446 387 216.88 2.422 328 216.25 2.415 290 215.88 2.411 285 214.38 2.394 371 210.56 2.352 114 209.38 2.338 104 122.81 1.372 1000
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