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4-Chlorobenzenamine hydrochloride

Product Name 4-Chlorobenzenamine hydrochloride

CAS20265-96-7

MFC6H7Cl2N

MW164.03

¹³CNMR

Mass

MS-NW-9317          
p-chloroaniline hydrochloride
C6H6ClN HCl         (Mass of molecular ion:    127)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      28.0       1.1
      35.0       1.2
      36.0      15.2
      37.0       1.0
      38.0       5.2
      39.0       2.9
      41.0       1.7
      44.5       1.0
      45.5       5.7
      52.0       1.4
      62.0       1.5
      63.0       3.4
      63.5       5.4
      64.0       3.8
      64.5       1.7
      65.0      16.3
      66.0       1.9
      73.0       2.3
      75.0       1.5
      90.0       1.6
      91.0       3.9
      92.0      15.3
      93.0       1.1
      99.0       4.9
     100.0       9.5
     101.0       2.2
     102.0       3.0
     126.0       2.0
     127.0     100.0
     128.0       7.8
     129.0      32.4
     130.0       2.3

90 MHz in D2O

¹H NMR	89.56 MHz
C₆ H₆ Cl N	0.040 g : 0.5 ml D₂O
p-chloroaniline hydrochloride

    Assign.     Shift(ppm)

      A             7.52
      B             7.39
     
     THE SOLVENT SIGNAL REMOVED.

     Hz     ppm     Int.

    680.38   7.597    277
    679.81   7.591    180
    677.75   7.568    169
    673.88   7.525    263
    671.31   7.496   1000
    669.19   7.472    261
    666.50   7.442    274
    664.38   7.419    967
    661.81   7.390    256
    657.88   7.346    175
    655.88   7.324    194
    655.19   7.316    261

in D2O

KBr disc

nujol mull

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