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2,6-Dimethoxybenzoyl chloride

Product Name 2,6-Dimethoxybenzoyl chloride

CAS1989-53-3

MFC9H9ClO3

MW200.62

Mass

MS-IW-3733          
2,6-dimethoxybenzoyl chloride
C9H9ClO3            (Mass of molecular ion:    200)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      36.0       2.3
      37.0       1.0
      38.0       1.3
      39.0       2.3
      50.0       2.5
      51.0       4.3
      52.0       1.0
      53.0       1.8
      55.0       1.1
      62.0       1.7
      63.0       3.7
      64.0       2.8
      65.0       1.4
      75.0       1.2
      76.0       2.4
      77.0       6.7
      78.0       1.3
      79.0       2.8
      82.5       1.5
      91.0       1.5
      92.0       4.6
     107.0      13.2
     108.0       1.1
     122.0       8.1
     135.0       1.7
     150.0      16.0
     151.0       1.5
     165.0     100.0
     166.0      10.2
     167.0       1.0
     200.0       4.2
     202.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₉ Cl O₃	0.042 g : 0.5 ml CDCl₃
2,6-dimethoxybenzoyl chloride

    Assign.     Shift(ppm)

      A             7.345
      B             6.573
      C             3.864

     Hz     ppm     Int.

   2943.88   7.367     34
   2935.64   7.346     67
   2927.70   7.326     39
   2630.92   6.584    131
   2622.53   6.563    122
   1544.49   3.865   1000

KBr disc

nujol mull

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