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2-CHLOROPHENETHYLALCOHOL

Product Name 2-CHLOROPHENETHYLALCOHOL

CAS19819-95-5

MFC8H9ClO

MW156.61

¹³CNMR

Mass

MS2014-05018CW      
o-chlorophenethyl alcohol
C8H9ClO             (Mass of molecular ion:    156)

   Source Temperature: 250 °C
   Sample Temperature: 200 °C
   Reservoir, 70 eV

      18.0       1.0
      28.0       4.6
      31.0       4.6
      32.0       1.8
      38.0       1.2
      39.0       5.7
      50.0       3.4
      51.0       5.7
      61.0       1.0
      62.0       3.4
      63.0      11.7
      64.0       2.5
      65.0       7.1
      73.0       2.8
      74.0       2.1
      75.0       3.8
      76.0       1.1
      77.0       5.4
      78.0       1.0
      86.0       1.0
      87.0       1.0
      89.0      28.8
      90.0      10.0
      91.0     100.0
      92.0       8.1
      99.0       8.3
     101.0       3.2
     102.0       2.1
     103.0       3.8
     112.0       1.4
     120.0       3.0
     121.0       1.4
     125.0      97.5
     126.0      61.4
     127.0      35.1
     128.0      19.9
     129.0       1.5
     137.0       1.1
     138.0       1.7
     156.0      42.2
     157.0       3.9
     158.0      13.7
     159.0       1.2
     205.0       1.1

in CDCl3

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₉ Cl O	0.05 ml : 0.5 ml CDCl₃
o-chlorophenethyl alcohol

    Assign.     Shift(ppm)

      A             7.299
      B             7.207
      C             7.136
      D             7.104
      E             3.763
      F             3.24
      G             2.940
     
     90MHZ : HSP-06-123

     Hz     ppm     Int.

   2927.98   7.327     30
   2926.39   7.323     37
   2922.00   7.312    387
   2920.41   7.308    345
   2914.43   7.293    490
   2912.72   7.289    467
   2890.01   7.232     36
   2885.74   7.221    271
   2883.91   7.217    349
   2878.42   7.203    379
   2876.34   7.198    459
   2870.36   7.183     33
   2868.16   7.177     37
   2867.07   7.174     37
   2866.46   7.173     38
   2865.36   7.170     39
   2861.82   7.161    217
   2860.23   7.157    255
   2856.69   7.148     60
   2854.49   7.143    495
   2852.91   7.139    476
   2849.12   7.130     65
   2847.17   7.125    373
   2845.34   7.120    590
   2843.14   7.115    398
   2837.77   7.101    383
   2835.69   7.096    382
   2831.79   7.086     44
   2830.20   7.082    155
   2828.25   7.077    137
   1524.66   3.815     33
   1522.46   3.810     30
   1517.70   3.798     58
   1511.11   3.782    485
   1504.15   3.764    842
   1497.19   3.747    484
   1490.60   3.730     36
   1296.39   3.244    162
   1195.31   2.991     36
   1188.48   2.974     59
   1181.76   2.957    615
   1174.80   2.940   1000
   1167.85   2.923    543
   1161.25   2.906     36

¹H NMR	89.56 MHz
C₈ H₉ Cl O	0.05 ml : 0.5 ml CDCl₃
o-chlorophenethyl alcohol

    Assign.     Shift(ppm)

      A          7.37 to 7.06
      B             3.774
      C             2.97
      D             2.958
     
     400MHZ : HSP-42-170

     Hz     ppm     Int.

    660.25   7.373    127
    659.31   7.362    130
    657.44   7.341    113
    654.75   7.311    286
    651.31   7.273    294
    650.44   7.263    328
    646.75   7.222    318
    645.56   7.209    428
    643.63   7.187    694
    641.88   7.168   1000
    639.19   7.138    391
    636.63   7.109    247
    635.13   7.092    221
    632.25   7.060    176
    628.75   7.021     50
    345.50   3.858    227
    338.69   3.782    506
    331.88   3.706    331
    282.25   3.152     32
    281.56   3.144     33
    270.69   3.023    505
    263.94   2.948    784
    257.06   2.871    329

in CDCl3

liquid film

4880 A,200 M,liquid

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