(S)-1,2,3,4-TETRAHYDROISOQUINOLINE-3-METHANOL
Product Name (S)-1,2,3,4-TETRAHYDROISOQUINOLINE-3-METHANOL
CAS18881-17-9
MFC10H13NO
MW163.22
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MassMS-KW-0531 (S)-1,2,3,4-tetrahydro-3-isoquinolinemethanol C10H13NO (Mass of molecular ion: 163)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.0 28.0 2.3 39.0 1.9 50.0 1.0 51.0 3.0 52.0 1.2 63.0 1.4 64.0 1.0 64.5 1.2 65.0 3.4 65.5 3.9 66.0 2.4 77.0 6.4 78.0 4.0 79.0 2.0 89.0 1.0 91.0 2.3 102.0 1.3 103.0 6.7 104.0 10.8 105.0 7.3 115.0 5.6 116.0 1.7 117.0 7.0 118.0 1.1 130.0 27.9 131.0 4.8 132.0 100.0 133.0 10.7 144.0 1.9 162.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C10H13NO 0.039 g : 0.5 ml CDCl3 (S)-1,2,3,4-tetrahydro-3-isoquinolinemethanol 
Assign. Shift(ppm)
A *1 7.12 B *1 7.10 C 7.056 D 6.986 E 4.00 F *2 3.724 G 3.57 J *2 3.502 K 3.009 L *3 2.540 M *3 2.588 assigned by C-H COSY
Hz ppm Int.2856.08 7.145 42 2853.89 7.139 75 2848.88 7.127 335 2847.42 7.123 446 2843.63 7.113 929 2840.09 7.105 700 2838.26 7.100 505 2833.38 7.088 133 2830.94 7.082 91 2828.37 7.075 82 2824.47 7.065 353 2820.93 7.057 302 2817.63 7.048 149 2815.56 7.043 193 2796.88 6.996 324 2791.26 6.982 265 2788.09 6.975 224 1617.80 4.047 43 1600.22 4.003 1000 1583.99 3.963 51 1496.71 3.744 289 1492.92 3.735 308 1485.60 3.717 373 1481.94 3.707 364 1426.64 3.569 700 1408.45 3.524 383 1400.88 3.505 412 1397.47 3.496 317 1389.90 3.477 328 1216.44 3.043 81 1211.92 3.032 114 1208.26 3.023 135 1205.69 3.016 162 1202.15 3.008 164 1201.05 3.005 164 1198.13 2.997 155 1194.46 2.988 123 1189.95 2.977 85 1070.20 2.677 89 1065.56 2.666 110 1053.72 2.636 331 1049.08 2.625 296 1043.22 2.610 273 1032.48 2.583 225 1026.98 2.569 85 1016.24 2.542 80
in CDCl3
KBr disk
Nujol
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