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18856-69-4

N,N-DIMETHYLAMINOMETHYLENEMALONIC ACID DIMETHYL ESTER

Product Name N,N-DIMETHYLAMINOMETHYLENEMALONIC ACID DIMETHYL ESTER

CAS18856-69-4

MFC8H13NO4

MW187.19

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  • 18856-69-4_ms_1
    Mass

    MS-IW-3621          
    dimethyl ((dimethylamino)methylene)malonate
    C8H13NO4            (Mass of molecular ion:    187)
    

       Source Temperature: 120 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          15.0       8.2
          18.0       1.0
          27.0       2.0
          28.0       4.1
          29.0       1.4
          39.0       1.3
          41.0       8.1
          42.0      33.7
          43.0      23.7
          44.0       7.5
          45.0      20.8
          52.0       1.2
          53.0       7.4
          54.0       1.5
          55.0       6.0
          59.0       6.5
          67.0       2.7
          68.0      14.1
          69.0      19.6
          70.0       3.6
          72.0       7.0
          81.0       1.7
          82.0       3.9
          83.0       5.2
          84.0       1.4
          85.0       2.1
          87.0       2.5
          88.0      14.2
          95.0       1.7
          96.0       7.6
          97.0      24.1
          98.0      11.5
          99.0       1.5
         100.0       1.3
         112.0       3.0
         113.0       5.3
         114.0       1.7
         124.0      89.9
         125.0      17.3
         126.0       6.6
         127.0       1.7
         128.0      14.8
         129.0       1.3
         140.0       6.8
         142.0       2.6
         155.0      41.9
         156.0     100.0
         157.0       8.5
         187.0      45.5
         188.0       4.5
    

400 MHz in CDCl3

  • 18856-69-4_1hnmr_0

    1H NMR 399.65 MHz
    C8 H13 N O4 0.047 g : 0.5 ml CDCl3
    dimethyl ((dimethylamino)methylene)malonate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.557 B *1 3.774 C *1 3.703 D 3.01

         Hz     ppm     Int.
    

       3020.14   7.557   1000
       1508.42   3.775    574
       1480.10   3.704    571
       1203.13   3.011    311
    

in CDCl3

  • 18856-69-4_13cnmr_0

KBr disc

  • 18856-69-4_ir1_2

nujol mull

  • 18856-69-4_ir2_1

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