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MassMS-NW-8599 tris(2-ethylhexyl)amine C24H51N (Mass of molecular ion: 353)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 1.0 29.0 3.4 30.0 2.5 41.0 6.8 42.0 2.7 43.0 11.9 44.0 9.7 55.0 5.4 56.0 1.4 57.0 14.8 58.0 6.7 69.0 3.5 70.0 1.6 71.0 6.4 72.0 3.6 84.0 2.3 98.0 1.3 112.0 3.8 126.0 2.8 140.0 2.6 142.0 6.6 154.0 4.3 156.0 19.6 157.0 2.3 252.0 1.1 254.0 100.0 255.0 19.3 256.0 1.8
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C24 H51 N 0.05 ml : 0.5 ml CDCl3 tris(2-ethylhexyl)amine 
Assign. Shift(ppm)
A 2.04 B 1.44 C 1.36 to 1.26 D 0.89 E 0.83
Hz ppm Int.191.38 2.137 32 182.69 2.040 257 181.81 2.031 261 181.56 2.028 261 181.44 2.026 261 175.38 1.959 51 173.75 1.941 41 172.69 1.929 36 172.13 1.922 34 171.44 1.915 32 170.94 1.909 30 146.06 1.631 30 145.31 1.623 33 145.00 1.620 32 144.19 1.610 34 143.75 1.606 35 143.38 1.601 34 142.88 1.596 34 142.50 1.592 36 141.94 1.585 39 141.63 1.582 39 140.56 1.570 43 139.69 1.560 47 139.19 1.555 50 138.44 1.546 52 136.69 1.527 64 136.19 1.521 64 135.06 1.509 70 129.31 1.444 139 128.69 1.437 144 112.56 1.257 1000 98.44 1.100 108 98.13 1.096 107 96.69 1.080 99 96.38 1.077 99 94.13 1.052 104 92.81 1.037 99 92.63 1.035 99 91.88 1.026 100 84.25 0.941 353 80.00 0.894 851 74.63 0.834 639 69.25 0.774 182 68.44 0.765 178 62.13 0.694 37
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1H NMR 399.65 MHz C24 H51 N 0.05 ml : 0.5 ml CDCl3 tris(2-ethylhexyl)amine Assign. Shift(ppm)
A 2.04 B 1.40 to 1.20 C 0.893 D 0.834 NLCI P427
Hz ppm Int.827.88 2.072 37 821.17 2.055 201 818.73 2.049 231 815.31 2.041 290 813.11 2.035 240 806.52 2.019 44 804.08 2.012 33 567.99 1.422 40 565.55 1.416 41 563.11 1.410 50 560.91 1.404 69 558.59 1.398 67 555.66 1.391 74 553.59 1.386 93 550.66 1.378 99 548.58 1.373 117 541.14 1.355 178 533.08 1.334 234 528.08 1.322 202 526.37 1.318 200 523.32 1.310 219 515.75 1.291 315 512.33 1.282 350 510.25 1.277 340 508.06 1.272 364 505.00 1.264 370 503.17 1.260 337 496.09 1.242 234 493.16 1.234 194 487.06 1.219 270 482.18 1.207 191 479.61 1.201 180 476.56 1.193 136 372.68 0.933 46 369.02 0.924 59 363.77 0.911 427 361.94 0.906 280 357.06 0.894 1000 349.85 0.876 546 340.45 0.852 351 333.37 0.835 713 326.05 0.816 388
in CDCl3
liquid film
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