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MassMS2006-02927WA 2-chloro-3-methylpyridine C6H6ClN (Mass of molecular ion: 127)
Source Temperature: 250 °C Sample Temperature: 250 °C Reservoir, 70 eV
18.0 1.0 26.0 1.6 27.0 1.9 37.0 4.2 38.0 7.4 39.0 20.8 40.0 2.7 41.0 2.3 49.0 1.2 50.0 3.8 51.0 4.4 52.0 2.8 61.0 2.7 62.0 4.5 62.5 1.3 63.0 12.4 63.5 1.1 64.0 17.0 65.0 36.1 66.0 5.7 73.0 2.6 75.0 1.6 76.0 1.7 90.0 4.0 91.0 89.3 92.0 56.1 93.0 3.8 99.0 2.8 100.0 1.3 101.0 1.4 126.0 5.8 127.0 100.0 128.0 8.6 129.0 32.0 130.0 2.2
in CDCl3
parameter in CDCl3
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1H NMR 300 MHz C6 H6 Cl N 20 % in CDCl3 2-chloro-3-methylpyridine 
Parameter ppm Hz
D(A) 8.18 D(B) 7.08 D(C) 7.52 D(D) 2.30 J(A,B) 4.8 J(A,C) 2.2 J(A,D) 0.6 J(B,C) 7.8 J(B,D) 0.3 J(C,D) 0.8 BELL,C.L. ET AL. J.HETEROCYCL.CHEM. 2, 420 (1965)
Hz ppm Int.2457.83 8.193 87 2457.28 8.191 91 2455.64 8.185 95 2455.09 8.184 93 2453.02 8.177 94 2452.47 8.175 96 2450.83 8.169 95 2450.28 8.168 92 2261.50 7.538 76 2260.73 7.536 83 2260.08 7.534 67 2259.37 7.531 81 2258.55 7.528 75 2253.73 7.512 85 2252.91 7.510 92 2252.20 7.507 75 2251.55 7.505 91 2250.78 7.503 84 2130.20 7.101 131 2125.38 7.085 131 2122.43 7.075 115 2117.62 7.059 109 690.05 2.300 1000
in CDCl3
Liquid film
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