5,5'-THIODISALICYLIC ACID

Mass

MS-NW-2164          
5,5'-thiodisalicylic acid
C14H10O6S           (Mass of molecular ion:    306)

   Source Temperature: 230 °C
   Sample Temperature: 250 °C
   Direct, 75 eV

      12.0       2.3
      16.0       4.3
      17.0       3.8
      18.0      13.8
      26.0       1.4
      27.0       4.6
      28.0      11.5
      29.0       2.4
      37.0       2.3
      38.0       6.7
      39.0      24.4
      40.0       1.9
      43.0       1.5
      44.0      71.0
      45.0      17.7
      47.0       1.1
      50.0       4.6
      51.0       7.0
      52.0       2.1
      53.0      15.1
      54.0       1.1
      55.0       4.2
      58.0       1.0
      61.0       2.7
      62.0       8.7
      63.0      26.8
      64.0       7.3
      65.0      11.1
      66.0       3.9
      67.0       1.9
      69.0      15.2
      70.0       9.6
      71.0       4.6
      72.0       1.4
      74.0       2.1
      75.0       2.2
      76.0       1.1
      77.0       3.0
      78.0       1.3
      79.0       8.4
      79.5       1.4
      80.0       1.6
      81.0       8.2
      82.0       1.8
      85.0       4.7
      85.5       1.2
      86.0       1.6
      87.0       1.0
      89.0       3.4
      90.0       1.3
      91.0       3.5
      92.0       5.6
      93.0       3.4
      93.5       2.1
      94.0      12.5
      94.5       1.0
      95.0      23.5
      96.0       5.3
      97.0       9.3
      98.0       4.6
      99.0       1.0
     100.0       1.5
     101.0       1.0
     102.0       1.9
     107.0       2.4
     108.0       2.8
     109.0       1.5
     114.0       2.9
     115.0      14.5
     116.0       3.1
     117.0       1.0
     118.0       3.4
     119.0       1.3
     120.0       2.9
     121.0       1.9
     122.0       6.8
     123.0       2.6
     124.0       2.8
     125.0       8.8
     126.0       5.5
     127.0       4.3
     128.0       4.0
     129.0       1.3
     131.0       6.3
     132.0       1.3
     133.0       1.2
     134.0       1.7
     135.0       2.8
     137.0       4.5
     138.0       1.3
     139.0       1.0
     143.0       1.4
     144.0       6.8
     145.0       2.2
     147.0       1.1
     150.0       1.1
     151.0       4.1
     152.0       1.8
     155.0      11.4
     156.0       2.6
     157.0       6.6
     158.0      11.3
     159.0       5.6
     160.0       3.0
     161.0       1.9
     162.0       1.7
     163.0       2.8
     169.0       1.2
     170.0       1.5
     171.0      13.2
     172.0       2.1
     173.0       1.6
     176.0       4.5
     183.0       2.6
     184.0       2.8
     185.0       5.1
     186.0      10.0
     187.0      37.4
     188.0      57.3
     189.0      11.8
     190.0       3.7
     191.0       2.3
     199.0       3.7
     200.0       2.6
     201.0       2.6
     202.0       1.2
     203.0       1.2
     214.0       9.5
     215.0       5.0
     216.0       5.9
     217.0       7.9
     218.0      35.7
     219.0       5.6
     220.0       2.4
     243.0       5.0
     244.0     100.0
     245.0      15.5
     246.0       6.8
     261.0       1.8
     262.0      75.1
     263.0      11.2
     264.0       5.2
     270.0      14.1
     271.0       3.0
     272.0       1.1
     288.0      12.4
     289.0       2.4
     290.0       1.0
     306.0      10.6
     307.0       1.7
     308.0       1.0

Assign. Shift(ppm) A 11. B 7.779 C 7.513 D 7.005

     Hz     ppm     Int.

   3110.35   7.783    975
   3107.97   7.777   1000
   3104.31   7.768     27
   3008.51   7.528    651
   3005.95   7.522    643
   2999.72   7.506    714
   2997.34   7.500    729
   2803.73   7.016    990
   2799.70   7.006     31
   2798.78   7.004     33
   2795.12   6.994    935