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MS-IW-4060 (octyloxy)benzene C14H22O (Mass of molecular ion: 206)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.3 29.0 3.6 39.0 1.6 41.0 8.3 42.0 1.7 43.0 11.4 51.0 1.0 55.0 6.3 56.0 2.6 57.0 8.7 65.0 2.0 66.0 1.5 69.0 3.4 70.0 3.0 71.0 4.7 77.0 5.3 79.0 1.0 83.0 1.8 94.0 100.0 95.0 8.2 107.0 1.8 206.0 13.5 207.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H22 O 0.05 ml : 0.5 ml CDCl3 (octyloxy)benzene Assign. Shift(ppm)
A 7.247 B 6.90 C 6.88 D 3.915 E 1.758 F 1.441 G 1.32 J 1.28 K 0.885
Hz ppm Int.
2907.10 7.275 54 2904.79 7.269 376 2902.59 7.263 135 2899.78 7.256 74 2897.46 7.250 524 2896.00 7.247 506 2893.68 7.241 85 2890.75 7.234 165 2888.79 7.229 466 2886.35 7.223 72 2766.85 6.924 112 2765.87 6.921 212 2764.77 6.918 150 2758.54 6.903 377 2757.57 6.900 249 2755.49 6.895 111 2753.30 6.890 524 2752.20 6.887 622 2751.34 6.885 438 2750.12 6.882 264 2746.58 6.873 174 2745.48 6.870 279 2744.51 6.868 536 2743.53 6.865 420 2740.97 6.859 72 1571.53 3.933 467 1564.94 3.916 908 1558.35 3.900 483 717.29 1.795 95 710.69 1.779 258 703.61 1.761 297 702.27 1.758 232 695.68 1.741 296 689.09 1.725 130 589.84 1.476 47 583.25 1.460 128 581.67 1.456 121 576.17 1.442 193 567.99 1.422 160 561.04 1.404 76 549.80 1.376 42 541.50 1.355 120 539.79 1.351 129 531.37 1.330 308 527.71 1.321 350 523.56 1.311 487 518.31 1.297 430 514.89 1.289 445 512.33 1.282 543 361.21 0.904 319 359.13 0.899 232 354.37 0.887 1000 347.29 0.869 395
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