TRI-N-BUTYLSULFONIUM IODIDE

Mass

MS-IW-7693          
tributylsulfonium iodide
C12H27IS            (Mass of molecular ion:    330)

   Source Temperature: 180 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      17.0       1.4
      18.0       4.9
      26.0       2.6
      27.0      15.6
      28.0       6.1
      29.0      47.4
      30.0       1.7
      35.0       1.1
      38.0       1.2
      39.0      10.0
      40.0       2.3
      41.0      56.6
      42.0       4.0
      43.0       3.6
      45.0       4.1
      46.0       3.2
      47.0       8.5
      48.0       2.1
      49.0       2.3
      50.0       1.3
      51.0       1.5
      53.0       3.3
      54.0       2.4
      55.0      23.1
      56.0      88.5
      57.0     100.0
      58.0       5.6
      59.0       1.8
      60.0       3.9
      61.0      84.4
      62.0       3.9
      63.0       4.4
      75.0       5.5
      88.0       3.4
      89.0      13.6
      90.0      35.1
      91.0      18.6
      92.0       2.9
      93.0       1.1
     103.0      17.8
     104.0       2.3
     105.0       1.1
     117.0       7.5
     127.0       3.5
     128.0       1.7
     141.0       1.2
     145.0       1.0
     146.0      66.1
     147.0       6.7
     148.0       3.7
     155.0       4.9
     184.0      62.9
     185.0       3.2

Assign. Shift(ppm) A 3.753 B 1.836 C 1.570 D 1.010

     Hz     ppm     Int.

   1508.18   3.774    239
   1500.37   3.755    232
   1498.54   3.750    144
   1492.55   3.735    254
    749.51   1.876     53
    743.53   1.861     79
    742.07   1.857    107
    739.75   1.851     84
    736.69   1.844     85
    734.13   1.837    199
    731.20   1.830     87
    726.56   1.818    136
    724.37   1.813     93
    718.75   1.799     71
    646.12   1.617     38
    638.67   1.599    134
    631.23   1.580    206
    623.66   1.561    202
    616.21   1.542    126
    608.89   1.524     36
    410.89   1.029    502
    403.56   1.010   1000
    396.12   0.992    458