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MassMS-NW-9391 2,6-difluorobenzamide C7H5F2NO (Mass of molecular ion: 157)
Source Temperature: 270 °C Sample Temperature: 160 °C Reservoir, 75 eV
18.0 2.7 28.0 1.8 31.0 2.4 37.0 1.6 39.0 1.0 44.0 10.4 50.0 3.1 51.0 1.0 56.0 1.0 57.0 2.6 61.0 2.3 62.0 4.1 63.0 22.8 64.0 1.8 64.5 1.2 68.0 3.5 69.0 1.9 70.0 1.0 74.0 2.8 75.0 2.3 81.0 2.2 87.0 1.3 88.0 2.7 92.0 1.2 93.0 3.6 94.0 2.6 101.0 1.2 112.0 2.5 113.0 37.5 114.0 8.7 139.0 4.6 140.0 1.0 141.0 100.0 142.0 7.6 157.0 50.4 158.0 4.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H5 F2 N O 0.038 g : 0.5 ml DMSO-d6 2,6-difluorobenzamide 
Assign. Shift(ppm)
A *1 8.16 B *1 7.87 C 7.488 D 7.150
Hz ppm Int.3262.02 8.163 242 3146.06 7.873 250 3007.97 7.527 153 3001.25 7.510 314 2999.27 7.505 238 2994.69 7.494 203 2992.86 7.489 581 2991.03 7.485 215 2986.45 7.473 236 2985.99 7.472 246 2984.31 7.468 358 2977.75 7.451 170 2870.03 7.182 115 2868.65 7.178 160 2865.60 7.171 845 2861.48 7.160 156 2860.26 7.157 204 2857.82 7.151 1000 2857.21 7.150 945 2854.92 7.144 217 2853.55 7.141 155 2849.58 7.131 738 2846.22 7.122 152 2845.15 7.120 109
in DMSO-d6
KBr disc
nujol mull
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