3,5-DIBROMOSALICYLAMIDE

Mass

MS-NW-9939          
3,5-dibromosalicylamide
C7H5Br2NO2          (Mass of molecular ion:    293)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      17.0       1.8
      18.0      10.0
      28.0       2.6
      37.0       2.0
      38.0       1.6
      39.0       1.1
      44.0       7.8
      44.5       1.1
      45.0       1.0
      50.0       1.5
      51.0       1.6
      52.0       1.7
      53.0       4.2
      53.5       4.5
      61.0       6.2
      62.0      13.2
      63.0      10.3
      64.0       1.8
      74.0       1.7
      78.0       1.3
      79.0       1.5
      80.0       2.3
      82.0       2.2
      85.0       1.5
      86.0       1.1
      88.0       1.0
      89.0       1.2
      90.0       3.3
      91.0       3.8
      92.0       1.2
     107.0       2.6
     108.0       2.2
     117.0       1.4
     119.0       1.3
     125.0       1.1
     141.0       8.1
     142.0       1.7
     143.0       8.8
     144.0       1.4
     147.5       1.1
     158.0       1.0
     169.0       2.4
     170.0       3.8
     171.0       2.5
     172.0       2.8
     197.0       9.3
     198.0       2.6
     199.0       9.2
     200.0       2.0
     220.0       3.0
     221.0       1.4
     222.0       5.9
     223.0       2.6
     224.0       2.9
     225.0       1.2
     248.0       5.6
     249.0       1.3
     250.0      10.6
     251.0       1.4
     252.0       5.3
     275.0       1.0
     276.0      51.3
     277.0       6.8
     278.0     100.0
     279.0      10.2
     280.0      49.3
     281.0       4.6
     293.0      21.8
     294.0       1.9
     295.0      42.4
     296.0       3.6
     297.0      20.8
     298.0       1.7

Assign. Shift(ppm) A 14.3 B *1 8.74 C *1 8.34 D 8.166 E 7.967

     Hz     ppm     Int.

   5717.12  14.306   1000
   3492.24   8.739    179
   3334.33   8.344    186
   3264.88   8.170    824
   3262.74   8.164    890
   3185.17   7.970   1000
   3182.82   7.965    953
   3180.47   7.959     55