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MS-NW-9709 3-pyridyl acetate C7H7NO2 (Mass of molecular ion: 137)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.3 28.0 1.6 38.0 2.7 39.0 9.6 40.0 3.6 41.0 2.8 42.0 1.6 43.0 57.4 44.0 1.4 50.0 1.1 51.0 1.9 55.0 1.4 66.0 3.1 67.0 5.1 68.0 4.5 94.0 1.4 95.0 100.0 96.0 7.9 109.0 5.8 137.0 21.2 138.0 3.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H7 N O2 0.05 ml : 0.5 ml CDCl3 3-pyridyl acetate Assign. Shift(ppm)
A 8.464 B 8.436 C 7.469 D 7.307 E 2.296
Hz ppm Int.
3385.74 8.472 107 3384.52 8.469 109 3381.10 8.461 109 3379.76 8.457 109 3372.68 8.440 141 3370.12 8.433 141 2991.70 7.486 87 2990.23 7.483 90 2989.01 7.480 86 2987.55 7.476 84 2983.40 7.466 107 2981.93 7.462 109 2980.59 7.459 109 2979.25 7.455 102 2926.76 7.324 113 2926.39 7.323 109 2922.00 7.312 110 2921.63 7.311 107 2918.46 7.303 90 2917.97 7.302 87 2913.70 7.291 87 2913.21 7.290 84 920.41 2.304 66 917.60 2.297 1000
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