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MS-NW-8078 tricyclohexylmethanol C19H34O (Mass of molecular ion: 278)
Source Temperature: 130 °C Sample Temperature: 100 °C Direct, 75 eV
18.0 1.8 29.0 1.6 41.0 8.2 43.0 1.6 53.0 1.1 55.0 18.3 57.0 1.3 67.0 7.4 69.0 2.2 79.0 2.1 81.0 17.8 82.0 2.0 83.0 18.4 84.0 1.3 91.0 1.1 93.0 1.6 95.0 45.0 96.0 4.3 97.0 2.3 99.0 5.7 109.0 4.6 110.0 1.2 111.0 4.7 113.0 4.8 121.0 4.4 135.0 3.8 176.0 1.4 177.0 17.8 178.0 4.9 194.0 2.0 195.0 100.0 196.0 14.3 197.0 1.2 260.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C19 H34 O 0.035 g : 0.5 ml CDCl3 tricyclohexylmethanol Assign. Shift(ppm)
A 1.76 B 1.66 C 1.19 to 1.14 ASSIGNED BY CH-COSY.
Hz ppm Int.
706.30 1.768 726 704.47 1.763 722 701.54 1.756 742 682.74 1.709 59 682.25 1.708 58 681.88 1.707 58 678.47 1.698 71 674.80 1.689 120 667.97 1.672 273 665.65 1.666 276 663.33 1.660 333 661.13 1.655 350 500.73 1.253 58 488.28 1.222 179 474.49 1.188 543 466.06 1.167 1000 456.91 1.144 322 454.59 1.138 372 451.29 1.130 606 442.26 1.107 155 435.18 1.089 43 432.62 1.083 45 429.69 1.076 39
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