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MS-NW-3332 (allyloxy)benzene C9H10O (Mass of molecular ion: 134)
Source Temperature: 290 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.3 26.0 1.4 27.0 4.1 37.0 1.7 38.0 5.3 39.0 37.6 40.0 4.0 41.0 100.0 42.0 3.4 43.0 1.2 50.0 4.0 51.0 12.2 52.0 1.9 53.0 1.0 54.0 1.0 55.0 3.4 62.0 1.7 63.0 5.2 64.0 2.3 65.0 19.0 66.0 10.9 68.0 3.1 74.0 1.1 77.0 15.0 78.0 12.2 79.0 7.1 80.0 1.0 91.0 20.9 92.0 5.1 93.0 2.4 94.0 33.2 95.0 2.3 103.0 1.8 105.0 10.8 106.0 3.7 107.0 3.4 115.0 2.5 116.0 2.5 117.0 3.1 119.0 16.2 120.0 1.6 131.0 1.7 133.0 17.2 134.0 64.3 135.0 6.6 174.0 1.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O 0.04 ml : 0.5 ml CDCl3 (allyloxy)benzene Assign. Shift(ppm)
A 7.25 B 7.03 to 6.78 C 6.03 D 5.40 E 5.28 F 4.518
Hz ppm Int.
660.06 7.371 202 659.06 7.359 299 657.06 7.337 179 654.50 7.308 81 653.69 7.299 201 652.75 7.289 400 652.19 7.283 321 651.56 7.276 478 650.75 7.267 388 649.94 7.258 486 648.56 7.242 192 647.38 7.229 186 645.75 7.211 350 645.06 7.203 243 644.06 7.192 605 643.31 7.184 807 641.19 7.160 177 628.81 7.022 128 627.94 7.012 197 627.19 7.004 301 626.31 6.994 479 624.81 6.977 255 622.88 6.955 764 621.81 6.943 1000 620.31 6.927 453 619.63 6.919 723 617.56 6.896 105 616.31 6.882 235 615.75 6.876 246 614.44 6.861 557 613.81 6.854 429 613.13 6.847 569 611.63 6.830 166 610.31 6.815 81 562.19 6.278 98 556.94 6.219 194 551.94 6.163 211 546.75 6.105 235 544.94 6.085 175 541.75 6.050 139 539.69 6.027 319 534.63 5.970 381 529.50 5.913 394 524.50 5.857 262 493.69 5.513 182 492.13 5.495 440 490.31 5.475 618 488.81 5.458 270 478.63 5.345 228 477.31 5.330 496 476.75 5.324 270 475.88 5.314 348 475.50 5.310 429 474.88 5.303 374 474.19 5.295 265 473.06 5.283 337 471.50 5.265 161 468.56 5.232 145 467.13 5.216 339 465.31 5.196 345 463.94 5.181 178 408.63 4.563 548 407.25 4.548 980 405.75 4.531 595 403.50 4.506 534 402.06 4.490 963 400.56 4.473 552
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