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17231-95-7

2,3-DICHLOROTHIOPHENOL

Product Name 2,3-DICHLOROTHIOPHENOL

CAS17231-95-7

MFC6H4Cl2S

MW179.07

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  • 17231-95-7_ms
    Mass

    MS-NW-9419          
    2,3-dichlorobenzenethiol
    C6H4Cl2S            (Mass of molecular ion:    178)
    

       Source Temperature: 250 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          36.0       3.2
          37.0       3.5
          38.0       2.6
          39.0       2.8
          44.0       1.9
          45.0       7.8
          49.0       1.8
          50.0       2.9
          51.0       1.0
          52.5       1.6
          53.0       8.3
          53.5       1.6
          54.0       1.3
          57.0       1.6
          58.0       3.3
          60.0       1.0
          61.0       3.8
          62.0       5.7
          63.0      11.1
          68.0       1.0
          69.0      14.7
          70.0       1.3
          71.0      11.4
          71.5       1.3
          72.0       5.2
          73.0       6.6
          74.0       6.9
          75.0       5.7
          79.0       4.6
          81.0       6.5
          82.0       5.4
          83.0       1.4
          84.0       3.5
          85.0       1.7
          86.0       1.0
          89.0       5.0
          90.0       3.3
          91.0       1.0
          92.0       1.0
          93.0       1.5
          97.0       3.2
          99.0       7.0
         101.0       2.0
         103.0       2.5
         105.0       2.6
         106.0       3.6
         107.0      26.7
         108.0      26.8
         109.0       8.3
         110.0       2.4
         111.0       2.2
         116.0       1.3
         118.0       2.5
         133.0       2.6
         134.0       6.7
         135.0       1.9
         136.0       4.3
         142.0      36.4
         143.0      88.5
         144.0      20.8
         145.0      34.0
         146.0       5.7
         147.0       2.5
         148.0       1.7
         177.0       5.6
         178.0     100.0
         179.0      11.0
         180.0      68.2
         181.0       5.7
         182.0      13.2
    

400 MHz in CDCl3

  • 17231-95-7_1hnmr

    1H NMR 399.65 MHz
    C6 H4 Cl2 S 0.027 g : 0.5 ml CDCl3
    2,3-dichlorobenzenethiol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.23 B 7.042 C 4.00

         Hz     ppm     Int.
    

       2895.87   7.247     85
       2894.41   7.243    701
       2893.19   7.240     99
       2891.85   7.236     35
       2890.14   7.232     23
       2886.84   7.224    786
       2886.47   7.223    793
       2821.78   7.061    314
       2814.09   7.042    296
       2813.48   7.040    286
       2805.91   7.021    208
       1600.22   4.005   1000
    

in CDCl3

  • 17231-95-7_13cnmr

KBr disc

  • 17231-95-7_ir1_2

nujol mull

  • 17231-95-7_ir2