VANILLIN AZINE

Mass

MS-NW-7125          
vanillin azine
C16H16N2O4          (Mass of molecular ion:    300)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      15.0       1.3
      27.0       1.3
      28.0       1.1
      38.0       1.5
      39.0       7.0
      41.0       2.9
      50.0       3.2
      51.0       9.0
      52.0      14.8
      53.0       3.9
      55.0       3.9
      62.0       1.3
      63.0       5.0
      64.0       2.8
      65.0      12.9
      66.0       2.1
      67.0       2.5
      76.0       2.1
      77.0       5.6
      78.0       3.1
      79.0       6.1
      80.0       5.8
      81.0       3.5
      90.0       2.0
      91.0       1.6
      92.0       2.1
      93.0       4.1
      94.0       1.3
      95.0       1.6
     104.0       1.3
     105.0       2.6
     106.0       6.1
     107.0       4.9
     108.0       8.1
     109.0       4.0
     118.0       1.0
     119.0       1.1
     120.0       2.7
     121.0       4.1
     122.0       3.1
     123.0       7.9
     124.0       1.7
     133.0       1.1
     134.0       7.1
     135.0       6.0
     136.0       2.8
     137.0       2.8
     141.0       1.0
     148.0       1.3
     149.0       5.0
     150.0      14.0
     151.0       4.3
     152.0       1.6
     162.0       5.8
     163.0       1.1
     168.0       1.3
     169.0       2.3
     170.0       1.5
     175.0       1.5
     176.0       1.5
     177.0      50.5
     178.0       5.8
     185.0       1.1
     186.0       1.3
     196.0       1.5
     197.0       3.2
     198.0       1.8
     207.0       1.7
     211.0       3.5
     212.0       1.8
     213.0       2.0
     214.0       1.8
     215.0       1.2
     224.0       1.2
     225.0       2.1
     226.0       1.2
     227.0       2.3
     228.0       1.5
     229.0       1.7
     230.0       1.9
     239.0       1.7
     240.0       1.5
     241.0       2.2
     242.0       1.8
     243.0       1.2
     253.0       1.4
     255.0       1.1
     256.0       3.0
     257.0       3.0
     258.0      19.5
     259.0       3.2
     267.0       1.0
     269.0       2.3
     270.0       1.0
     271.0       1.6
     272.0      11.4
     273.0      16.4
     274.0       2.8
     283.0       2.1
     284.0       6.4
     285.0       6.8
     286.0       1.2
     299.0      32.6
     300.0     100.0
     301.0      18.5
     302.0       2.6

Assign. Shift(ppm) A 9.72 B 8.599 C 7.482 D 7.273 E 6.901 F 3.852

     Hz     ppm     Int.

   3883.36   9.717    282
   3436.89   8.600    371
   2991.33   7.485    193
   2989.50   7.481    201
   2912.14   7.287     97
   2910.31   7.283     98
   2903.90   7.267    108
   2902.07   7.262    107
   2762.15   6.912    211
   2754.06   6.892    208
   1539.76   3.853   1000