ACETIC ACID TRANS-2-HEPTEN-1-YL ESTER

Mass

MS-IW-2185          
trans-2-heptenyl acetate
C9H16O2             (Mass of molecular ion:    156)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       3.0
      27.0       9.8
      28.0       2.1
      29.0       6.6
      39.0      11.7
      40.0       1.8
      41.0      22.1
      42.0       6.9
      43.0     100.0
      44.0       4.6
      45.0       1.2
      51.0       1.1
      53.0       5.6
      54.0      45.0
      55.0      33.7
      56.0       5.1
      57.0      15.9
      58.0       3.4
      61.0       3.9
      65.0       1.2
      66.0       1.3
      67.0      20.3
      68.0       9.9
      69.0       4.9
      70.0       6.2
      71.0       8.8
      72.0       5.5
      73.0       2.0
      79.0       1.4
      81.0      25.8
      82.0       1.9
      83.0       1.3
      85.0       3.4
      86.0       2.2
      95.0       4.7
      96.0      27.4
      97.0       5.2
      98.0       1.1
      99.0       3.7
     100.0       3.1
     113.0       5.5
     114.0      18.1
     115.0       1.6
     156.0       1.0

Assign. Shift(ppm) A 5.766 B 5.563 C 4.502 D 2.05 E 2.048 F 1.37 G 1.32 J 0.897 ASSIGNED BY C-H COSY. J(A,B)=15.4HZ

     Hz     ppm     Int.

   2313.35   5.789     44
   2304.69   5.767     35
   2299.07   5.753     37
   2297.97   5.750     64
   2296.88   5.748     37
   2291.26   5.734     34
   2236.57   5.597     36
   2231.45   5.584     39
   2230.10   5.581     72
   2228.64   5.577     38
   2223.51   5.564     38
   2214.72   5.542     52
   1803.34   4.513    159
   1802.37   4.510    167
   1796.75   4.496    160
   1795.90   4.494    170
    833.62   2.086     60
    832.52   2.084     41
    825.93   2.067    182
    818.48   2.048   1000
    812.50   2.034     65
    557.13   1.395     44
    553.83   1.386     48
    549.80   1.376     79
    548.58   1.373     67
    546.02   1.367     65
    542.36   1.358     98
    541.02   1.354     77
    539.67   1.351     88
    536.62   1.343    103
    533.33   1.335     56
    530.88   1.329     79
    529.66   1.326     93
    526.00   1.317     49
    524.17   1.312     55
    522.58   1.308     70
    516.97   1.294     33
    514.65   1.288     39
    365.36   0.915    219
    362.18   0.907     35
    358.28   0.897    381
    351.07   0.879    163