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16851-72-2

N-(P-TOLUENESULFONYL)-3-PYRROLINE

Product Name N-(P-TOLUENESULFONYL)-3-PYRROLINE

CAS16851-72-2

MFC11H13NO2S

MW223.29

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  • 16851-72-2_ms
    Mass

    MS-IW-9069          
    1-(p-tolylsulfonyl)-3-pyrroline
    C11H13NO2S          (Mass of molecular ion:    223)
    

       Source Temperature: 150 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          27.0       1.0
          28.0       3.1
          39.0      11.3
          40.0       2.2
          41.0      19.9
          42.0       2.3
          50.0       1.1
          51.0       2.3
          63.0       3.5
          64.0       1.1
          65.0      15.6
          66.0       1.1
          67.0       7.6
          68.0     100.0
          69.0       5.0
          77.0       1.2
          89.0       3.5
          90.0       2.1
          91.0      72.6
          92.0      14.3
          93.0       1.0
         107.0       1.4
         108.0       1.3
         139.0       2.5
         155.0      31.0
         156.0       3.4
         157.0       1.9
         158.0       1.8
         222.0       8.9
         223.0      31.4
         224.0       4.8
         225.0       1.8
    

400 MHz in DMSO-d6

  • 16851-72-2_1hnmr

    1H NMR 399.65 MHz
    C11 H13 N O2 S 0.036 g : 0.5 ml DMSO-d6
    1-(p-tolylsulfonyl)-3-pyrroline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.715 B 7.435 C 5.710 D 4.015 E 2.393

         Hz     ppm     Int.
    

       3089.97   7.732     39
       3088.01   7.727    240
       3086.43   7.723     89
       3081.54   7.711     94
       3079.83   7.707    291
       3077.88   7.702     51
       2975.59   7.446    215
       2967.65   7.426    186
       2967.04   7.425    180
       2286.50   5.722     40
       2282.23   5.711    460
       2277.71   5.700     39
       1609.01   4.027     57
       1604.74   4.016   1000
       1600.34   4.005     54
        956.67   2.394    706
    

in DMSO-d6

  • 16851-72-2_13cnmr

KBr disc

  • 16851-72-2_ir1_2

nujol mull

  • 16851-72-2_ir2