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MS-IW-9011 2,3-diphenylquinoxaline C20H14N2 (Mass of molecular ion: 282)
Source Temperature: 160 °C Sample Temperature: 120 °C Direct, 75 eV
28.0 1.2 50.0 9.5 51.0 4.0 63.0 1.1 74.0 1.2 75.0 3.4 76.0 17.7 77.0 8.2 102.0 2.0 103.0 3.0 126.0 1.7 127.0 1.8 128.0 1.7 140.0 13.4 140.5 11.5 141.0 19.2 151.0 5.9 152.0 7.0 153.0 3.8 176.0 1.5 177.0 4.0 178.0 19.7 179.0 38.7 180.0 5.7 205.0 3.5 279.0 1.8 281.0 64.0 282.0 100.0 283.0 21.0 284.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H14 N2 0.041 g : 0.5 ml CDCl3 2,3-diphenylquinoxaline Assign. Shift(ppm)
A 8.177 B 7.753 C 7.522 D 7.33
Hz ppm Int.
3276.98 8.200 34 3275.88 8.197 44 3272.95 8.190 346 3269.53 8.181 307 3266.60 8.174 277 3263.06 8.165 384 3260.13 8.158 47 3259.16 8.156 39 3106.81 7.774 42 3105.83 7.772 52 3102.78 7.764 360 3099.49 7.756 267 3096.44 7.748 289 3093.02 7.740 344 3090.09 7.732 43 3088.99 7.730 33 3014.04 7.542 56 3011.11 7.535 441 3009.52 7.531 485 3008.06 7.527 247 3007.08 7.525 212 3005.62 7.521 205 3004.15 7.517 401 3003.54 7.516 445 3001.46 7.511 542 2946.90 7.374 48 2945.19 7.370 48 2940.06 7.357 158 2938.84 7.354 193 2936.04 7.347 244 2935.18 7.345 377 2933.35 7.340 1000 2931.27 7.335 463 2929.57 7.331 200 2927.61 7.326 284 2926.03 7.322 474 2925.54 7.321 448 2923.95 7.317 97 2922.97 7.314 91 2921.88 7.312 95 2920.29 7.308 139 2918.82 7.304 75 2917.11 7.300 95
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