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TRILAURYL TRITHIOPHOSPHITE

Product Name TRILAURYL TRITHIOPHOSPHITE

CAS1656-63-9

MFC36H75PS3

MW635.15

¹³CNMR

Mass

MS-NW-5441          
tridodecyl trithiophosphite
C36H75PS3           (Mass of molecular ion:    634)

   Source Temperature: 190 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      27.0      17.4
      28.0       3.9
      29.0      35.2
      39.0      14.1
      40.0       2.5
      41.0      72.6
      42.0      13.8
      43.0     100.0
      44.0       3.6
      45.0       3.9
      46.0       1.2
      47.0       8.4
      53.0       5.7
      54.0       7.0
      55.0      61.7
      56.0      21.8
      57.0      92.4
      58.0       4.2
      59.0       2.0
      60.0       5.6
      61.0       5.9
      63.0       4.4
      65.0       1.1
      67.0      10.5
      68.0       8.1
      69.0      37.4
      70.0      16.3
      71.0      44.5
      72.0       2.7
      73.0       2.4
      74.0       1.0
      79.0       1.5
      81.0       5.8
      82.0       7.9
      83.0      22.5
      84.0      10.0
      85.0      25.3
      86.0       1.9
      87.0      12.7
      88.0       2.2
      89.0       4.9
      95.0       3.3
      96.0       4.4
      97.0      15.0
      98.0       6.5
      99.0       6.8
     101.0       6.8
     103.0       1.1
     105.0       1.3
     109.0       1.5
     110.0       1.7
     111.0       6.9
     112.0       3.6
     113.0       4.4
     115.0       2.8
     119.0       1.0
     125.0       2.9
     126.0       1.8
     127.0       2.2
     129.0       2.1
     139.0       1.3
     140.0       2.9
     143.0       1.6
     145.0       1.6
     157.0       1.2
     159.0       1.1
     168.0       5.5
     169.0       1.6
     173.0       1.7
     187.0       1.2
     199.0       4.7
     200.0       7.3
     201.0      62.3
     202.0      14.6
     203.0       4.7
     229.0       3.3
     230.0       1.0
     231.0       5.5
     232.0       1.7
     233.0       1.3
     234.0       1.4
     263.0       1.0
     264.0       3.6
     265.0       8.1
     266.0       1.9
     267.0       1.4
     297.0       1.5
     298.0       1.7
     299.0       1.2
     402.0       3.6
     403.0       1.2
     432.0       1.5
     433.0      16.7
     434.0       5.5
     435.0       2.4
     465.0       1.0
     466.0       2.1
     467.0       1.3
     634.0       3.9
     635.0       1.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₃₆ H₇₅ P S₃	0.04 ml : 0.5 ml CDCl₃
tridodecyl trithiophosphite

    Assign.     Shift(ppm)

      A             2.81
      B             1.70
      C             1.26
      D             0.89

     Hz     ppm     Int.

    126.44   1.412     34
    124.19   1.387     45
    121.56   1.358     57
    112.88   1.261   1000
     84.13   0.940     45
     81.88   0.915     36
     81.25   0.908     35
     78.94   0.882    146
     72.94   0.815     32

in CDCl3

CCl4 solution

liquid film

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