1,2-PHENYLENE PHOSPHOROCHLORIDITE

Mass

MS-IW-3732          
o-phenylene phosphorochloridite
C6H4ClO2P           (Mass of molecular ion:    174)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      26.0       1.6
      37.0       1.1
      38.0       3.4
      39.0       1.2
      47.0       5.3
      50.0       3.3
      51.0       3.5
      52.0       4.2
      53.0       1.6
      57.0       1.0
      62.0       2.3
      63.0      10.5
      64.0       7.9
      66.0       1.4
      69.5       1.9
      83.0       1.8
      92.0      27.8
      93.0       1.9
     139.0     100.0
     140.0       6.8
     174.0      34.4
     175.0       2.3
     176.0      11.2

Assign. Shift(ppm) A 7.219 B 7.096 J(A,P-31)=0.8HZ

     Hz     ppm     Int.

   2895.51   7.246     50
   2894.65   7.243     86
   2893.68   7.241     63
   2890.87   7.234    538
   2889.89   7.232    504
   2887.45   7.225    574
   2886.47   7.223    540
   2884.64   7.218    489
   2884.16   7.217    441
   2883.79   7.216    430
   2881.47   7.210    693
   2880.62   7.208    678
   2877.44   7.200    123
   2876.95   7.199    130
   2876.59   7.198    128
   2876.10   7.197    104
   2844.73   7.119    152
   2844.36   7.118    159
   2840.33   7.108   1000
   2836.91   7.099    688
   2834.35   7.093    796
   2830.93   7.084    785
   2827.15   7.075     97
   2826.29   7.072     80