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MS-NW-8546 1,10-diiododecane C10H20I2 (Mass of molecular ion: 394)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
18.0 1.2 27.0 19.0 28.0 2.9 29.0 24.6 39.0 13.8 40.0 2.5 41.0 77.8 42.0 10.2 43.0 79.8 44.0 2.7 53.0 4.9 54.0 3.1 55.0 100.0 56.0 8.7 57.0 78.0 58.0 3.5 67.0 4.7 68.0 1.6 69.0 55.0 70.0 5.1 71.0 44.8 72.0 2.5 81.0 2.8 83.0 60.2 84.0 4.4 85.0 15.7 86.0 1.1 91.0 1.6 97.0 25.4 98.0 2.1 99.0 1.6 107.0 1.2 109.0 1.0 127.0 1.5 128.0 1.4 135.0 3.2 137.0 2.9 139.0 8.8 140.0 1.0 141.0 1.1 149.0 1.6 151.0 1.5 155.0 15.8 163.0 2.1 165.0 2.1 169.0 9.0 177.0 1.3 179.0 1.2 183.0 9.6 197.0 7.2 211.0 7.3 225.0 3.7 267.0 6.3 394.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H20 I2 0.05 ml : 0.5 ml CDCl3 1,10-diiododecane Assign. Shift(ppm)
A 3.178 B 1.82 C 1.40 D 1.29
Hz ppm Int.
292.25 3.264 104 285.31 3.186 257 278.44 3.109 152 169.69 1.895 74 169.25 1.890 73 168.94 1.887 72 168.25 1.879 71 163.00 1.821 121 156.44 1.747 103 156.13 1.744 102 151.38 1.691 46 150.63 1.682 46 150.25 1.678 46 149.75 1.673 46 144.31 1.612 24 143.94 1.608 23 143.31 1.601 23 142.75 1.594 23 115.94 1.295 1000
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