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MassMS-NW-9349 1,6-dibromo-2-naphthol C10H6Br2O (Mass of molecular ion: 300)
Source Temperature: 160 °C Sample Temperature: 150 °C Direct, 75 eV
18.0 2.0 55.0 1.0 56.0 5.0 56.5 4.7 57.0 3.1 62.0 1.6 63.0 3.6 70.5 1.8 71.0 4.3 86.0 1.4 87.0 1.9 88.0 1.5 96.0 2.6 96.5 3.6 97.0 2.9 97.5 3.4 110.0 1.4 111.0 1.4 113.0 13.6 114.0 6.3 141.0 4.0 142.0 2.0 150.0 4.8 151.0 9.4 151.5 1.0 152.0 4.7 192.0 10.0 193.0 5.9 194.0 10.3 195.0 5.5 222.0 1.4 224.0 1.0 273.0 1.4 300.0 51.1 301.0 6.0 302.0 100.0 303.0 11.1 304.0 49.5 305.0 5.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H6 Br2 O 0.049 g : 0.5 ml CDCl3 1,6-dibromo-2-naphthol 
Assign. Shift(ppm)
A 7.885 B 7.841 C 7.590 D 7.580 E 7.238 F 5.92
Hz ppm Int.3152.34 7.888 730 3150.39 7.883 754 3138.67 7.854 571 3129.64 7.831 670 3038.09 7.602 539 3034.55 7.594 561 3032.59 7.589 550 3029.30 7.580 618 3025.51 7.571 474 3023.56 7.566 465 2896.97 7.249 1000 2888.18 7.227 849 2364.87 5.918 823
in CDCl3
KBr disc
nujol mull
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