3-Quinuclidinol

Mass

MS-NW-2156          
3-quinuclidinol
C7H13NO             (Mass of molecular ion:    127)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       4.8
      18.0       2.6
      27.0       7.6
      28.0       3.9
      29.0       4.5
      30.0       8.4
      31.0       1.4
      39.0       5.5
      40.0       1.0
      41.0      11.7
      42.0     100.0
      43.0      28.3
      44.0       9.4
      53.0       2.5
      54.0       3.0
      55.0       9.2
      56.0       8.1
      57.0      10.4
      58.0      26.2
      59.0       1.0
      67.0       1.8
      68.0       3.9
      69.0       6.0
      70.0      12.9
      71.0       4.4
      72.0       2.8
      73.0       4.3
      80.0       1.1
      81.0       1.5
      82.0      11.0
      83.0       6.9
      84.0       4.7
      85.0       1.1
      86.0       2.5
      96.0       8.5
      97.0       1.9
      98.0      12.1
      99.0       5.2
     108.0       1.1
     109.0       1.0
     110.0       5.9
     112.0       6.8
     126.0       7.5
     127.0      37.8
     128.0       3.1

Assign. Shift(ppm) A 4.5 B 3.791 C *1 3.087 D *2 2.886 E *2 2.75 F *2 2.628 G *1 2.570 J *3 1.951 K 1.783 L *4 1.671 M *4 1.458 N *3 1.349 ASSIGNED BY H-H COSY.

     Hz     ppm     Int.

   1784.55   4.466    127
   1520.26   3.804    641
   1518.92   3.801    681
   1516.60   3.795    457
   1515.38   3.792    680
   1514.28   3.790    498
   1511.84   3.783    674
   1510.62   3.780    702
   1246.34   3.119    467
   1244.02   3.113    490
   1238.04   3.098    470
   1235.72   3.093    505
   1232.30   3.084    557
   1229.98   3.078    577
   1224.00   3.063    493
   1221.68   3.057    513
   1157.84   2.898    464
   1155.15   2.891    482
   1152.22   2.884    488
   1109.86   2.778    465
   1108.03   2.773    426
   1104.61   2.764    488
   1102.05   2.758    662
   1099.24   2.751    762
   1097.17   2.746    728
   1096.07   2.743    724
   1092.77   2.735    555
   1090.21   2.728    524
   1088.26   2.724    503
   1085.82   2.717    538
   1052.37   2.634    492
   1049.80   2.627    520
   1047.36   2.621    487
   1036.25   2.593    692
   1033.57   2.587    841
   1030.52   2.579    506
   1022.09   2.558    459
   1019.17   2.551    637
   1016.48   2.544    424
    784.06   1.962    367
    781.37   1.956    460
    778.56   1.949    462
    776.12   1.942    394
    717.65   1.796    546
    714.36   1.788    980
    711.18   1.780   1000
    708.01   1.772    585
    679.44   1.701    333
    674.32   1.688    335
    671.26   1.680    461
    669.19   1.675    379
    667.60   1.671    416
    666.26   1.668    506
    662.60   1.658    384
    661.25   1.655    398
    657.35   1.645    340
    656.13   1.642    368
    596.44   1.493    341
    593.63   1.486    348
    590.70   1.479    365
    586.06   1.467    513
    583.25   1.460    582
    580.32   1.453    561
    577.64   1.446    430
    535.77   1.341    385
    528.20   1.322    221