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MassMS-NW-8577 1-piperidinecarbonitrile C6H10N2 (Mass of molecular ion: 110)
Source Temperature: 250 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 2.5 26.0 3.0 27.0 15.6 28.0 24.9 29.0 10.9 30.0 1.9 38.0 1.2 39.0 16.2 40.0 4.0 41.0 45.2 42.0 100.0 43.0 27.7 44.0 2.8 51.0 1.5 52.0 1.2 53.0 10.6 54.0 13.2 55.0 48.6 56.0 13.8 57.0 22.3 65.0 1.5 67.0 11.2 68.0 6.8 69.0 56.1 70.0 4.4 81.0 3.8 82.0 9.6 83.0 3.5 92.0 2.2 95.0 4.6 109.0 53.7 110.0 73.8 111.0 9.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H10 N2 0.05 ml : 0.5 ml CDCl3 1-piperidinecarbonitrile 
Assign. Shift(ppm)
A 3.19 B 1.68 C 1.61
Hz ppm Int.295.81 3.303 38 295.31 3.298 45 287.81 3.214 431 285.50 3.188 612 280.00 3.127 461 273.69 3.056 45 272.69 3.045 37 162.44 1.814 39 161.31 1.802 44 158.88 1.775 77 157.81 1.763 78 156.25 1.745 99 152.88 1.708 262 149.69 1.672 426 146.56 1.637 800 145.31 1.623 1000 143.75 1.606 940 141.94 1.585 818 134.63 1.504 64 134.31 1.500 59 132.63 1.481 40 132.06 1.475 38 131.38 1.467 37
in CDCl3
liquid film
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