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MassMS-IW-0038 9,9'-bifluorene C26H18 (Mass of molecular ion: 330)
Source Temperature: 210 °C Sample Temperature: 140 °C Direct, 75 eV
115.0 1.0 139.0 1.4 163.0 3.2 164.0 3.7 165.0 100.0 166.0 15.6 167.0 1.1 330.0 15.7 331.0 4.5
400 MHz at 65C
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1H NMR 399.65 MHz C26 H18 0.031 g : 0.5 ml CDCl3 at 60 C 9,9'-bifluorene 
Assign. Shift(ppm)
A 7.640 B *1 7.229 C *1 7.046 D 6.930 E 4.798
Hz ppm Int.3043.82 7.617 599 3042.97 7.615 891 3042.11 7.612 664 3039.67 7.606 52 3036.25 7.598 688 3035.40 7.596 1000 3034.55 7.594 740 2897.34 7.250 409 2896.36 7.248 432 2892.33 7.238 58 2889.89 7.232 832 2888.92 7.229 885 2885.38 7.220 54 2882.32 7.213 465 2881.35 7.210 488 2878.66 7.203 49 2824.58 7.068 476 2823.49 7.065 494 2820.68 7.058 46 2817.02 7.049 942 2815.92 7.046 983 2812.99 7.039 64 2812.26 7.037 66 2809.57 7.031 557 2808.47 7.028 565 2804.81 7.019 33 2772.95 6.939 701 2765.26 6.920 530 2758.79 6.904 31 1917.60 4.799 927
(at 50.C)
KBr disc
nujol mull
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