1,2-CYCLODODECANEDIOL

Mass

MS-IW-9344          
1,2-cyclododecanediol
C12H24O2            (Mass of molecular ion:    200)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.2
      18.0       4.1
      19.0       1.5
      27.0      16.6
      28.0       8.5
      29.0      34.1
      30.0       1.7
      31.0      10.6
      39.0      14.4
      40.0       3.0
      41.0      76.7
      42.0      18.3
      43.0      54.1
      44.0      20.5
      45.0       9.9
      47.0       1.0
      53.0       7.1
      54.0      25.2
      55.0      96.3
      56.0      28.2
      57.0      77.2
      58.0       9.6
      59.0       2.8
      60.0       1.8
      61.0       2.0
      65.0       1.4
      66.0       7.6
      67.0      56.8
      68.0      50.5
      69.0      49.6
      70.0      39.6
      71.0      23.8
      72.0       5.1
      73.0       4.1
      74.0       8.6
      75.0       2.9
      77.0       1.8
      78.0       1.5
      79.0      14.8
      80.0      20.0
      81.0      47.1
      82.0     100.0
      83.0      59.5
      84.0      23.6
      85.0      20.8
      86.0       4.3
      87.0       7.2
      91.0       1.3
      93.0      13.0
      94.0      16.0
      95.0      36.8
      96.0      54.2
      97.0      34.7
      98.0      26.9
      99.0       4.9
     100.0       2.8
     101.0      10.9
     107.0       9.3
     108.0       9.2
     109.0      13.8
     110.0      12.4
     111.0      14.0
     112.0       8.0
     113.0       2.2
     114.0       1.2
     115.0       2.8
     121.0      17.2
     122.0       8.2
     123.0       6.1
     124.0       4.5
     125.0       5.2
     126.0       5.8
     127.0       1.2
     135.0      12.4
     136.0       8.5
     137.0       2.1
     138.0       5.5
     139.0       3.1
     140.0       1.2
     149.0       1.7
     151.0       1.5
     152.0       1.0
     153.0       1.1
     154.0       1.3
     164.0       4.1
     165.0       1.0
     169.0       3.3
     182.0       3.4
     183.0       1.5

Assign. Shift(ppm) A 3.788 A 3.665 B 2.42 B 2.15 C 1.70 C 1.57 D 1.45 D 1.38 E 1.34 CIS-TRANS MIXTURE

     Hz     ppm     Int.

   1464.97   3.666    290
    966.67   2.419    103
    675.54   1.691    133
    628.66   1.574    149
    575.07   1.439    284
    550.17   1.377    852
    537.84   1.346   1000
    498.54   1.248     30