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ETHYLENE GLYCOL MONO-P-TOLYL ETHER

Product Name ETHYLENE GLYCOL MONO-P-TOLYL ETHER

CAS15149-10-7

MFC9H12O2

MW152.19

¹³CNMR

Mass

MS-NW-2386          
2-(p-tolyloxy)ethanol
C9H12O2             (Mass of molecular ion:    152)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.4
      27.0       5.2
      28.0       1.2
      29.0       4.3
      31.0       1.3
      39.0       5.3
      41.0       1.1
      43.0       2.8
      44.0       2.4
      45.0       8.3
      50.0       2.4
      51.0       5.0
      52.0       2.6
      53.0       2.8
      63.0       2.9
      65.0       7.7
      77.0      10.3
      78.0       2.7
      79.0       8.7
      80.0       5.9
      89.0       2.4
      90.0       6.5
      91.0      19.7
      92.0       1.8
      93.0       2.2
     107.0      53.2
     108.0     100.0
     109.0      10.3
     121.0       4.7
     152.0      35.3
     153.0       3.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₂ O₂	0.048 g : 0.5 ml CDCl₃
2-(p-tolyloxy)ethanol

    Assign.     Shift(ppm)

      A             7.05
      B             6.81
      C             4.01
      D             3.92
      E             2.43
      F             2.28

     Hz     ppm     Int.

    638.00   7.124    141
    637.38   7.117    164
    635.81   7.100     71
    635.13   7.092     61
    631.50   7.052     68
    630.94   7.045     79
    629.13   7.025    320
    628.56   7.019    290
    626.63   6.997     61
    626.06   6.991     56
    615.19   6.870     58
    612.69   6.842    447
    610.31   6.815    120
    606.13   6.768     76
    603.94   6.744    216
    366.50   4.093     50
    364.38   4.069     80
    363.44   4.059     75
    361.25   4.034    126
    360.19   4.022    130
    359.44   4.014    184
    357.19   3.989    378
    356.63   3.983    360
    353.69   3.950    371
    353.13   3.943    385
    350.94   3.919    182
    350.13   3.910    148
    349.13   3.899    129
    346.88   3.874     81
    346.00   3.864     81
    343.88   3.840     54
    217.50   2.429    462
    203.75   2.276   1000

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,200 M,powder

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