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1,3-Dimethoxybenzene

Product Name 1,3-Dimethoxybenzene

CAS151-10-0

MFC8H10O2

MW138.16

¹³CNMR

Mass

MS-NW-0816          
m-dimethoxybenzene
C8H10O2             (Mass of molecular ion:    138)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.3
      28.0       1.2
      38.0       3.5
      39.0       6.1
      41.0       8.3
      50.0       3.9
      51.0       5.2
      52.0       8.6
      53.0       1.5
      62.0       2.5
      63.0       9.4
      64.0       8.3
      65.0      15.6
      66.0       1.4
      67.0       2.4
      69.0       2.2
      74.0       1.3
      76.0       1.0
      77.0       9.1
      78.0      22.8
      79.0       7.1
      80.0       6.9
      92.0       6.9
      93.0       7.2
      94.0       3.7
      95.0      22.1
      96.0       1.5
     105.0       1.2
     107.0       6.0
     108.0      16.0
     109.0      29.7
     110.0       2.4
     123.0       1.1
     137.0       3.6
     138.0     100.0
     139.0       8.7

90 MHz in CDCl3

in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₀ O₂	0.05 ml : 0.5 ml CDCl₃
m-dimethoxybenzene

    Assign.     Shift(ppm)

      A             7.15
      B             6.50
      C             6.44
      D             3.741

     Hz     ppm     Int.

    643.19   7.182     21
    640.50   7.152     57
    634.69   7.087     22
    632.81   7.066     33
    586.00   6.544     73
    583.94   6.521     89
    583.44   6.515     90
    579.94   6.476     55
    576.88   6.442    198
    335.13   3.742   1000

in CDCl3

CCl4 solution

liquid film

4880 A,100M,liquid

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