TRANS-2-HYDROXYCYCLOHEXYLP-TOLUENESULFONATE

Mass

MS-NW-7910          
trans-2-hydroxycyclohexyl p-toluenesulfonate
C13H18O4S           (Mass of molecular ion:    270)

   Source Temperature: 180 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      17.0       1.3
      18.0       5.4
      19.0       1.3
      27.0       9.2
      28.0       2.1
      29.0       6.6
      31.0       5.0
      39.0      13.3
      40.0       2.0
      41.0      34.0
      42.0       6.2
      43.0       6.5
      44.0       2.3
      45.0       1.2
      47.0       1.7
      50.0       1.7
      51.0       3.8
      52.0       1.6
      53.0       3.6
      54.0       4.4
      55.0       7.9
      56.0       2.0
      57.0      11.9
      62.0       1.1
      63.0       4.9
      64.0       1.7
      65.0      23.0
      66.0       1.7
      67.0      13.1
      68.0       2.2
      69.0      34.6
      70.0      31.7
      71.0       2.9
      77.0       5.4
      78.0       1.4
      79.0      35.5
      80.0       6.7
      81.0       3.9
      83.0      11.1
      87.0       1.1
      89.0       5.6
      90.0       3.8
      91.0      63.6
      92.0      45.7
      93.0       5.4
      97.0      82.1
      98.0     100.0
      99.0       7.4
     107.0       8.7
     108.0       7.8
     115.0      43.6
     116.0       3.0
     121.0       1.2
     139.0       5.7
     155.0       8.8
     156.0       6.6
     157.0       7.6
     171.0       1.0
     172.0       8.7
     173.0       7.5
     174.0       1.1
     269.0       1.5

Assign. Shift(ppm) A 7.824 B 7.350 C 4.291 D 3.577 E 2.62 F 2.445 G 2.00 J 1.67 K *1 1.43 L *1 1.29 M 1.23

     Hz     ppm     Int.

   3134.28   7.843     53
   3132.32   7.838    336
   3130.74   7.834    149
   3125.73   7.822    115
   3123.78   7.817    373
   2943.73   7.366     45
   2941.77   7.361    235
   2941.04   7.360    297
   2940.43   7.358    235
   2939.09   7.355    124
   2935.18   7.345     80
   2933.11   7.340    269
   2932.50   7.338    271
   1727.54   4.323     53
   1722.66   4.311     57
   1718.99   4.302     61
   1716.55   4.296     65
   1714.23   4.290     68
   1711.67   4.283     62
   1708.01   4.274     61
   1703.13   4.262     58
   1440.19   3.604     40
   1435.67   3.593     59
   1431.52   3.582     49
   1430.05   3.579     56
   1427.12   3.571     63
   1425.17   3.567     63
   1421.51   3.557     42
   1416.63   3.545     47
   1045.65   2.617    119
    977.29   2.446   1000