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N-METHYLCARBAZOLE

Product Name N-METHYLCARBAZOLE

CAS1484-12-4

MFC13H11N

MW181.24

¹³CNMR

Mass

MS-IW-0797          
9-methylcarbazole
C13H11N             (Mass of molecular ion:    181)

   Source Temperature: 160 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      63.0       1.4
      75.0       1.0
      76.0       2.7
      77.0       2.8
      89.0       1.3
      89.5       1.1
      90.0       5.7
      90.5       7.0
      91.0       1.0
     139.0       2.1
     140.0       3.0
     151.0       3.2
     152.0      10.4
     153.0       3.4
     164.0       1.0
     166.0       4.2
     178.0       2.9
     179.0       1.6
     180.0      51.5
     181.0     100.0
     182.0      14.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₁ N	0.038 g : 0.5 ml CDCl₃
9-methylcarbazole

    Assign.     Shift(ppm)

      A             8.070
      B             7.437
      C             7.329
      D             7.208
      E             3.738

     Hz     ppm     Int.

   3229.37   8.081    142
   3228.64   8.079    180
   3221.56   8.061    152
   3220.83   8.060    191
   2981.69   7.461     83
   2980.47   7.458     81
   2974.49   7.443    115
   2973.39   7.440    204
   2972.29   7.438    124
   2966.31   7.423    143
   2965.09   7.420    135
   2932.74   7.339    237
   2924.56   7.318    168
   2888.55   7.228    125
   2887.57   7.226    116
   2880.62   7.208    205
   2873.66   7.191    107
   2872.68   7.188     98
   1494.02   3.739   1000

in CDCl3

KBr disc

nujol mull

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