3-BROMOCINNAMIC ACID

Mass

MS-NW-9714          
trans-3-bromocinnamic acid
C9H7BrO2            (Mass of molecular ion:    226)

   Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       3.7
      27.0       1.3
      37.0       1.0
      38.0       2.3
      39.0       4.2
      43.0       1.0
      45.0       3.3
      45.5       1.3
      49.0       1.9
      50.0      18.1
      50.5       1.1
      51.0      32.3
      51.5       1.5
      52.0       6.2
      53.0       1.5
      55.0       1.0
      59.0       4.8
      59.5       1.5
      61.0       1.9
      62.0       4.0
      63.0       8.0
      64.0       1.4
      65.0       8.5
      69.0       2.2
      71.0       1.8
      73.0       5.9
      73.5       9.3
      74.0      14.3
      75.0      28.2
      76.0      22.4
      77.0      12.5
      78.0       2.1
      79.0       4.5
      87.0       1.3
      89.0       4.1
      90.0       4.4
      90.5       1.4
      91.0      33.0
      91.5       1.4
      92.0       2.8
      98.0       2.5
      99.0       1.6
     100.0       1.5
     101.0      20.6
     102.0      81.4
     103.0      26.9
     104.0       2.2
     104.5       1.0
     118.0       8.5
     119.0       9.8
     129.0       1.8
     130.0       8.1
     131.0       1.2
     146.0       1.0
     147.0      62.4
     148.0       7.3
     155.0       2.1
     156.0       1.4
     157.0       3.1
     158.0       1.2
     159.0       1.1
     169.0       2.1
     171.0       2.1
     172.0       1.1
     180.0      10.1
     181.0      16.0
     182.0      11.4
     183.0      16.4
     184.0       2.6
     185.0       2.2
     187.0       1.1
     198.0       2.2
     199.0       1.0
     200.0       2.2
     208.0       5.4
     209.0      17.7
     210.0       7.1
     211.0      17.0
     212.0       1.7
     225.0      62.7
     226.0     100.0
     227.0      71.1
     228.0      98.0
     229.0       9.9

Assign. Shift(ppm) A 12.6 B 7.950 C 7.722 D 7.61 E 7.584 F 7.383 G 6.633

     Hz     ppm     Int.

   5015.64  12.551     73
   3179.04   7.955    466
   3177.39   7.951    797
   3175.74   7.947    502
   3090.57   7.734    392
   3082.69   7.714    444
   3045.33   7.620    302
   3044.59   7.619    340
   3043.49   7.616    337
   3042.58   7.614    317
   3038.92   7.604    752
   3037.45   7.601    489
   3036.53   7.598    459
   3035.44   7.596    445
   3034.70   7.594    374
   3022.98   7.565    754
   2958.32   7.403    509
   2954.48   7.393     52
   2950.45   7.383    843
   2942.57   7.363    395
   2658.84   6.653   1000
   2642.91   6.614    941