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2,4-Dibromo-1-fluorobenzene

Product Name 2,4-Dibromo-1-fluorobenzene

CAS1435-53-6

MFC6H3Br2F

MW253.89

¹³CNMR

Mass

MS-IW-0582          
2,4-dibromo-1-fluorobenzene
C6H3Br2F            (Mass of molecular ion:    252)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      31.0       1.5
      37.0       2.4
      38.0       1.2
      47.0       2.4
      49.0       1.5
      50.0       8.2
      61.0       3.0
      62.0       2.5
      63.0       1.7
      68.0       8.1
      73.0       2.4
      74.0       9.7
      75.0       3.6
      86.0       2.7
      86.5       1.3
      87.0       2.8
      87.5       1.3
      92.0       3.4
      93.0      11.6
      94.0      45.6
      95.0       3.1
     126.0       3.5
     127.0       6.8
     128.0       3.9
     153.0       1.0
     172.0       1.3
     173.0      37.1
     174.0       3.7
     175.0      36.2
     176.0       2.4
     252.0      51.2
     253.0       3.8
     254.0     100.0
     255.0       6.8
     256.0      48.6
     257.0       3.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₃ Br₂ F	0.05 ml : 0.5 ml CDCl₃
2,4-dibromo-1-fluorobenzene

    Assign.     Shift(ppm)

      A             7.657
      B             7.363
      C             6.980

     Hz     ppm     Int.

   3064.45   7.668    745
   3062.01   7.662    800
   3058.35   7.653    776
   3055.91   7.647    825
   2951.17   7.385    410
   2948.73   7.379    414
   2946.90   7.374    436
   2944.46   7.368    419
   2942.38   7.363    459
   2938.11   7.352    573
   2935.67   7.346    474
   2797.97   7.002    779
   2789.55   6.980   1000
   2789.18   6.980    938
   2783.20   6.965     27
   2781.01   6.959    736

in CDCl3

liquid film

4880 A,200 M,liquid

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