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MS-NW-1210 2,2'-(ethylimino)diethanol C6H15NO2 (Mass of molecular ion: 133)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.9 18.0 2.2 19.0 1.3 27.0 6.0 28.0 9.0 29.0 5.7 30.0 22.4 31.0 2.3 41.0 2.4 42.0 11.3 43.0 4.2 44.0 5.3 45.0 17.0 56.0 15.9 57.0 2.8 58.0 38.0 59.0 2.1 70.0 1.8 71.0 1.1 72.0 2.2 74.0 8.6 84.0 1.0 86.0 1.3 88.0 2.4 100.0 1.7 102.0 100.0 103.0 6.1 118.0 1.2 132.0 1.0 133.0 1.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H15 N O2 0.04 ml : 0.5 ml CDCl3 2,2'-(ethylimino)diethanol Assign. Shift(ppm)
A 3.83 B 3.606 C 2.640 D 2.628 E 1.045
Hz ppm Int.
343.31 3.834 653 328.75 3.671 514 325.81 3.638 106 323.50 3.613 900 320.56 3.580 114 317.94 3.551 665 246.44 2.752 111 241.25 2.694 647 239.13 2.671 498 235.69 2.632 840 232.00 2.591 509 230.56 2.575 509 225.19 2.515 145 100.19 1.119 480 96.69 1.080 24 95.38 1.065 33 93.25 1.042 1000 88.69 0.991 23 86.06 0.961 376
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