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N,N-DIMETHYL-4-NITROSOANILINE

Product Name N,N-DIMETHYL-4-NITROSOANILINE

CAS138-89-6

MFC8H10N2O

MW150.18

¹³CNMR

Mass

MS-NW-4763          
N,N-dimethyl-p-nitrosoaniline
C8H10N2O            (Mass of molecular ion:    150)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       4.6
      17.0       1.1
      18.0       5.5
      27.0       2.0
      28.0       2.0
      29.0       1.7
      30.0       3.3
      37.0       1.6
      38.0       2.9
      39.0       6.6
      40.0       1.2
      41.0       2.4
      42.0      36.0
      43.0       2.3
      44.0       4.2
      50.0       8.4
      51.0       8.4
      52.0       4.7
      53.0       2.3
      54.0       1.1
      61.0       1.0
      62.0       2.0
      63.0       8.6
      64.0       3.9
      65.0       7.0
      66.0       4.0
      67.0       1.3
      68.0       2.6
      69.0       1.7
      74.0       3.1
      75.0       2.9
      76.0       6.5
      77.0      35.7
      78.0      15.8
      79.0      20.2
      80.0       3.8
      81.0       1.4
      90.0       6.4
      91.0      17.2
      92.0      10.7
      93.0       5.8
      94.0       2.4
     102.0       1.0
     103.0       3.5
     104.0      22.3
     105.0      37.1
     106.0       3.8
     107.0       1.0
     117.0       2.3
     118.0      13.7
     119.0      26.4
     120.0      37.4
     121.0       5.2
     132.0       1.6
     133.0       2.5
     134.0       2.1
     135.0       2.1
     136.0       3.7
     147.0       2.1
     148.0       2.7
     150.0     100.0
     151.0      10.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₀ N₂ O	0.029 g : 0.5 ml CDCl₃
N,N-dimethyl-p-nitrosoaniline

    Assign.     Shift(ppm)

      A             7.79
      B             6.654
      C             3.138
     
     90MHZ : HSP-06-120 AT ROOM TEMP

     Hz     ppm     Int.

    702.69   7.847     27
    702.31   7.842     27
    701.63   7.835     26
    694.13   7.751     30
    693.50   7.744     31
    600.19   6.702     83
    599.00   6.689     42
    592.13   6.612     39
    590.75   6.597     68
    281.06   3.139   1000

in CDCl3

KBr disc

nujol mull

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