Di-o-tolythiourea

Mass

MS-NW-0475          
1,3-di(o-tolyl)-2-thiourea
C15H16N2S           (Mass of molecular ion:    256)

   Source Temperature: 210 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      27.0       3.2
      28.0       3.0
      30.0       1.8
      32.0       1.3
      33.0       1.0
      34.0       2.7
      38.0       1.9
      39.0      13.0
      40.0       1.3
      41.0       3.5
      45.0       4.1
      50.0       3.6
      51.0       8.5
      52.0       4.5
      53.0       2.6
      54.0       1.1
      62.0       1.9
      63.0       7.4
      64.0       3.1
      65.0      21.2
      66.0       1.9
      75.0       1.2
      76.0       1.5
      77.0      13.7
      78.0       7.8
      79.0       8.0
      80.0       2.7
      89.0       9.5
      90.0       7.4
      91.0      30.6
      92.0       3.3
      93.0       1.6
     103.0       1.1
     104.0       7.8
     105.0       2.5
     106.0      53.9
     107.0     100.0
     108.0       8.2
     116.0       6.7
     117.0      18.1
     118.0       3.5
     121.0       4.8
     122.0       1.6
     123.0       3.2
     124.0       7.0
     127.0       1.1
     128.0       1.1
     130.0       6.5
     131.0       4.2
     132.0       3.3
     133.0       6.0
     148.0       8.4
     149.0      27.9
     150.0      11.3
     151.0       2.4
     165.0       1.0
     204.0       1.9
     205.0       1.7
     206.0       2.7
     207.0       3.9
     208.0       1.0
     221.0      10.5
     222.0      25.9
     223.0      14.4
     224.0       2.4
     241.0      19.4
     242.0       3.6
     243.0       1.3
     255.0       5.5
     256.0      42.1
     257.0       7.9
     258.0       2.5

Assign. Shift(ppm) A 7.7 B 7.36 C 7.27 to 7.200 D 2.294 400MHZ : HSP-44-178

     Hz     ppm     Int.

    692.69   7.735     54
    667.06   7.449     28
    664.81   7.424     37
    662.75   7.401     57
    661.81   7.390     55
    659.56   7.365     93
    656.75   7.334    108
    654.63   7.310     81
    651.50   7.275    165
    649.06   7.248    625
    647.13   7.226    214
    645.75   7.211    264
    641.94   7.168     44
    639.94   7.146     52
    205.50   2.295   1000
    200.13   2.235     30