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MS-IW-8077 2-diethylamino-N-(2,6-xylyl)acetamide C14H22N2O (Mass of molecular ion: 234)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.0 28.0 1.6 29.0 2.6 30.0 6.3 42.0 2.4 56.0 2.5 57.0 1.0 58.0 7.4 72.0 4.7 77.0 1.8 84.0 1.0 86.0 100.0 87.0 7.1 91.0 1.6 105.0 1.0 120.0 2.5 234.0 5.5 235.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H22 N2 O 0.040 g : 0.5 ml CDCl3 2-diethylamino-N-(2,6-xylyl)acetamide Assign. Shift(ppm)
A 8.92 B 7.09 C 3.215 D 2.685 E 2.231 F 1.134
Hz ppm Int.
3566.41 8.924 25 2834.59 7.093 75 2831.91 7.086 426 1285.28 3.217 547 1084.11 2.713 124 1077.03 2.695 378 1069.82 2.677 384 1062.74 2.660 131 891.72 2.232 1000 460.21 1.152 423 453.13 1.134 782 445.92 1.116 399
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