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135540-11-3

1-(Chloro-1-pyrrolidinylmethylene)pyrrolidinium hexafluorophosphate

Product Name 1-(Chloro-1-pyrrolidinylmethylene)pyrrolidinium hexafluorophosphate

CAS135540-11-3

MFC9H16ClF6N2P

MW332.66

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  • 135540-11-3_ms_1
    Mass

    MS-IW-7236          
    1-(chloro(1-pyrrolidinyl)methylene)pyrrolidinium hexafluorophosphate
    C9H16ClF6N2P        (Mass of molecular ion:    332)
    

       Source Temperature: 180 °C
       Sample Temperature: 230 °C
       Direct, 75 eV
    

          15.0       2.4
          17.0       2.8
          18.0      14.1
          20.0       5.7
          26.0       1.7
          27.0       8.1
          28.0      18.6
          29.0       5.5
          30.0       8.1
          35.0       1.9
          36.0      20.4
          37.0       1.6
          38.0       7.2
          39.0      13.9
          40.0       8.3
          41.0      35.5
          42.0      17.7
          43.0      13.2
          44.0      15.0
          49.0       2.5
          50.0       1.5
          51.0       1.1
          53.0       3.0
          54.0       3.9
          55.0      73.5
          56.0      35.5
          57.0       1.7
          58.0       9.2
          60.0       1.0
          62.0       2.8
          64.0       1.3
          66.0       1.8
          67.0      16.0
          68.0      10.6
          69.0      19.4
          70.0     100.0
          71.0      11.1
          72.0       1.4
          76.0       3.7
          78.0       2.0
          81.0       1.0
          82.0       1.9
          83.0       1.7
          84.0       1.0
          85.0      43.3
          88.0       6.0
          89.0       1.2
          90.0       1.3
          91.0       1.7
          95.0       1.1
          96.0       2.2
          97.0       3.2
          98.0      63.2
          99.0      10.0
         104.0      49.8
         107.0      20.7
         112.0       1.0
         113.0       1.1
         117.0       1.2
         120.0       1.7
         125.0       8.0
         126.0       1.0
         129.0       3.2
         139.0       1.1
         140.0       5.4
         141.0       1.3
         145.0       2.9
         151.0       1.1
         153.0       1.1
         158.0       2.3
         160.0       1.0
         164.0       3.0
         168.0      34.3
         169.0       4.1
         171.0       1.3
         187.0       3.6
         189.0       1.1
    

400 MHz in CDCl3

  • 135540-11-3_1hnmr_0

    1H NMR 399.65 MHz
    C9 H16 Cl F6 N2 P 0.040 g : 0.5 ml CDCl3
    1-(chloro(1-pyrrolidinyl)methylene)pyrrolidinium hexafluorophosphate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 3.892 B 2.077

         Hz     ppm     Int.
    

       1562.03   3.909    338
       1555.62   3.893    833
       1549.21   3.877    367
        836.79   2.094    372
        832.94   2.085    493
        830.16   2.078   1000
        827.60   2.071    507
        823.54   2.061    385
    

in CDCl3

  • 135540-11-3_13cnmr_0

KBr disc

  • 135540-11-3_ir1_2

nujol mull

  • 135540-11-3_ir2_1