N-(2-Naphthyl)aniline

Mass

MS-NW-1721          
N-phenyl-2-naphthylamine
C16H13N             (Mass of molecular ion:    219)

   Source Temperature: 190 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       2.2
      50.0       1.2
      51.0       4.0
      63.0       2.2
      65.0       1.8
      75.0       1.6
      77.0       3.9
      89.0       1.8
      94.5       1.7
      95.5       3.0
      96.5       1.5
     101.0       1.5
     102.0       2.8
     107.5       1.3
     108.5      11.4
     109.0       4.0
     109.5       5.9
     110.0       1.0
     114.0       1.0
     115.0      10.1
     116.0       3.5
     126.0       2.2
     127.0       3.4
     128.0       1.0
     140.0       1.2
     153.0       1.1
     165.0       1.3
     178.0       1.0
     189.0       2.5
     190.0       1.5
     191.0       3.4
     192.0       2.8
     204.0       1.2
     216.0       4.6
     217.0      21.7
     218.0      34.3
     219.0     100.0
     220.0      17.5
     221.0       1.4

Assign. Shift(ppm) A 7.72 B 7.71 C 7.618 D 7.40 E 7.39 F 7.29 G 7.28 J 7.181 K 7.131 L 6.964 M 5.80 ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   3089.23   7.730    393
   3088.62   7.729    406
   3086.55   7.724    561
   3081.18   7.710    438
   3080.44   7.708    445
   3077.64   7.701    588
   3049.44   7.631    369
   3048.71   7.629    369
   3041.26   7.610    435
   3040.53   7.608    432
   2958.74   7.404    785
   2957.15   7.400    677
   2951.78   7.386    379
   2950.44   7.383    518
   2949.10   7.380    259
   2946.66   7.374     58
   2943.60   7.366    311
   2942.26   7.363    296
   2923.10   7.315    113
   2921.02   7.309    569
   2918.70   7.304    504
   2917.36   7.300    451
   2915.89   7.297    189
   2913.70   7.291    838
   2912.48   7.288    982
   2910.52   7.283    735
   2909.30   7.280    452
   2907.10   7.275    323
   2905.15   7.270    818
   2903.69   7.266    357
   2902.47   7.263    315
   2875.49   7.196    504
   2873.17   7.190    502
   2866.70   7.174    467
   2864.38   7.168    451
   2860.35   7.158     48
   2859.99   7.157     48
   2859.50   7.156     48
   2856.08   7.147    181
   2854.25   7.142    801
   2853.15   7.140   1000
   2851.07   7.134    303
   2847.53   7.126    274
   2846.56   7.123    442
   2845.70   7.121    749
   2844.60   7.118    659
   2842.29   7.112    121
   2791.50   6.985    211
   2790.41   6.983    382
   2789.31   6.980    216
   2787.60   6.976     45
   2786.74   6.973     49
   2784.42   6.968    285
   2784.06   6.967    294
   2783.08   6.964    641
   2782.10   6.962    295
   2776.86   6.949    193
   2775.76   6.946    320
   2774.66   6.943    169
   2316.04   5.796    273