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MS-NW-6870 phenoxazine C12H9NO (Mass of molecular ion: 183)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.6 39.0 1.7 50.0 2.8 51.0 3.9 52.0 2.4 63.0 3.0 64.0 1.9 74.0 1.3 75.0 1.6 76.0 1.8 77.0 4.4 78.0 1.6 91.0 1.3 91.5 8.5 92.0 1.4 101.0 1.2 102.0 1.4 126.0 1.5 127.0 5.5 128.0 4.1 129.0 1.8 153.0 2.1 154.0 22.1 155.0 5.5 182.0 17.5 183.0 100.0 184.0 13.5 185.0 1.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C12 H9 N O 0.036 g : 0.5 ml DMSO-d6 phenoxazine Assign. Shift(ppm)
A 8.20 B 6.731 C 6.608 D 6.574 E 6.470
Hz ppm Int.
3275.39 8.196 63 2698.97 6.754 321 2697.27 6.750 344 2691.89 6.736 490 2691.28 6.735 476 2690.06 6.732 534 2689.58 6.730 493 2684.20 6.717 448 2682.37 6.712 484 2647.58 6.625 308 2645.87 6.621 433 2639.65 6.605 1000 2637.94 6.601 870 2633.67 6.590 593 2632.20 6.587 618 2626.59 6.573 497 2625.12 6.569 505 2618.65 6.553 200 2617.19 6.549 208 2590.21 6.482 657 2588.87 6.478 628 2582.52 6.462 605 2581.05 6.459 555
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