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13380-94-4More Spectrum > TRICYCLO[5.2.1.02,6]DECAN-8-ONE(13380-94-4)MS
TRICYCLO[5.2.1.02,6]DECAN-8-ONE
Product Name TRICYCLO[5.2.1.02,6]DECAN-8-ONE
CAS13380-94-4
MFC10H14O
MW150.22
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MassMS-IW-0072 tricyclo(5.2.1.0(2,6))decane-8-one C10H14O (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 12.6 28.0 2.0 29.0 3.7 38.0 1.3 39.0 22.8 40.0 5.7 41.0 20.9 42.0 2.1 43.0 1.9 50.0 2.0 51.0 6.4 52.0 4.0 53.0 14.4 54.0 14.5 55.0 9.6 63.0 1.9 65.0 8.4 66.0 17.8 67.0 37.2 68.0 13.6 69.0 1.8 70.0 1.1 77.0 19.6 78.0 13.1 79.0 85.1 80.0 53.9 81.0 39.9 82.0 10.4 83.0 3.9 84.0 1.8 85.0 2.1 91.0 22.2 92.0 8.3 93.0 38.6 94.0 16.3 95.0 6.7 96.0 2.1 103.0 1.2 104.0 5.3 105.0 5.8 106.0 100.0 107.0 42.3 108.0 24.5 109.0 47.8 110.0 3.9 117.0 5.6 119.0 10.9 120.0 2.7 121.0 31.0 122.0 14.8 123.0 1.7 131.0 1.3 132.0 5.1 133.0 2.0 134.0 2.0 135.0 5.5 148.0 3.0 149.0 4.9 150.0 78.2 151.0 9.3 152.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H14 O 0.05 ml : 0.5 ml CDCl3 tricyclo(5.2.1.0(2,6))decane-8-one 
Assign. Shift(ppm)
A *1 2.403 B 2.360 C *1 2.12 D 2.021 E 1.98 F 1.78 G 1.77 to 1.75 J 1.529 K 1.347 L 1.09 ASSIGNED BY C-H COSY
Hz ppm Int.963.26 2.411 451 962.04 2.408 466 958.86 2.400 480 958.13 2.398 471 957.64 2.397 472 943.24 2.361 1000 857.91 2.147 311 852.29 2.133 417 849.12 2.125 621 845.70 2.117 456 840.33 2.103 365 831.42 2.081 118 822.88 2.060 327 818.36 2.048 319 805.66 2.016 538 801.27 2.005 487 799.07 2.000 277 797.61 1.996 309 795.90 1.992 300 794.43 1.988 249 790.65 1.979 336 789.06 1.975 357 787.60 1.971 336 786.25 1.968 305 785.03 1.965 369 783.69 1.961 368 781.86 1.957 333 777.95 1.947 235 776.37 1.943 295 774.90 1.939 283 767.94 1.922 141 723.14 1.810 620 718.75 1.799 877 715.33 1.790 311 714.84 1.789 309 709.11 1.775 557 704.35 1.763 624 701.54 1.756 817 698.36 1.748 419 696.17 1.742 347 618.77 1.549 193 617.31 1.545 470 615.97 1.542 596 614.50 1.538 413 613.04 1.534 167 609.74 1.526 133 608.03 1.522 164 606.57 1.518 330 605.10 1.515 469 603.64 1.511 365 602.17 1.507 163 564.45 1.413 106 557.74 1.396 176 551.88 1.381 300 545.29 1.365 496 539.43 1.350 365 532.84 1.334 528 526.37 1.318 288 520.39 1.303 255 517.21 1.295 31 513.92 1.286 137 457.89 1.146 136 455.20 1.139 59 450.93 1.129 264 445.07 1.114 332 443.36 1.110 300 438.35 1.097 437 437.26 1.095 410 431.76 1.081 386 430.66 1.078 428 425.78 1.066 249 423.95 1.061 322 417.85 1.046 196 413.94 1.036 54 411.01 1.029 98
in CDCl3
liquid film
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